2-[2'-(5-hexynoyloxy)ethylamino]-4,6-di(4'-methoxybenzylamino)-1,3,5-triazine

Base Information

Chemical Name:2-[2'-(5-hexynoyloxy)ethylamino]-4,6-di(4'-methoxybenzylamino)-1,3,5-triazine
CAS No.:1391054-29-7
Molecular Formula:C₂₇H₃₂N₆O₄
Molecular Weight:504.589
Hs Code.:

Synonyms:2-[2'-(5-hexynoyloxy)ethylamino]-4,6-di(4'-methoxybenzylamino)-1,3,5-triazine

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Chemical Property of 2-[2'-(5-hexynoyloxy)ethylamino]-4,6-di(4'-methoxybenzylamino)-1,3,5-triazine

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Technology Process of 2-[2'-(5-hexynoyloxy)ethylamino]-4,6-di(4'-methoxybenzylamino)-1,3,5-triazine

There total 2 articles about 2-[2'-(5-hexynoyloxy)ethylamino]-4,6-di(4'-methoxybenzylamino)-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 2-(2'-hydroxyethylamino)-4,6-di(4'-methoxybenzylamino)-1,3,5-triazine

: 53293-00-8
hex-5-ynoic acid

: 1391054-29-7
2-[2'-(5-hexynoyloxy)ethylamino]-4,6-di(4'-methoxybenzylamino)-1,3,5-triazine

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.bmc.2012.05.072

Reference yield:

: 2393-23-9
4-methoxy-benzylamine

: 1391054-29-7
2-[2'-(5-hexynoyloxy)ethylamino]-4,6-di(4'-methoxybenzylamino)-1,3,5-triazine

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetone / 0.33 h / 0 °C

1.2: 20 h / 20 °C

2.1: 1,4-dioxane / 60 h / 100 °C

3.1: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

With dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; acetone;
DOI:10.1016/j.bmc.2012.05.072

Reference yield: 73.0%

: 1391054-18-4
N-(6-azidocaproyl)deacetylcolchicine

: 1391054-29-7
2-[2'-(5-hexynoyloxy)ethylamino]-4,6-di(4'-methoxybenzylamino)-1,3,5-triazine

: 1391054-44-6
4-{4'-[3,5-di(4-methoxybenzylamino)-2,4,6-triazinylamino]ethyloxy-4'-oxobutyl}-1-{6'-[(1,2,3,10-tetramethoxy-9-oxo-5,6,7,9-tetrahydrobenzo[a]heptalen-7-yl)amino]-6'-oxohexyl}-1,2,3-triazole

Guidance literature:: With magnesium ascorbate; copper(II) sulfate; In tetrahydrofuran; water; at 20 ℃; for 24h;
DOI:10.1016/j.bmc.2012.05.072