Benzoic acid (2R,3S,5R)-5-(2-isobutyrylamino-6-oxo-1,6-dihydro-purin-9-yl)-2-methylsulfanylmethoxymethyl-tetrahydro-furan-3-yl ester

Base Information

• Chemical Name: Benzoic acid (2R,3S,5R)-5-(2-isobutyrylamino-6-oxo-1,6-dihydro-purin-9-yl)-2-methylsulfanylmethoxymethyl-tetrahydro-furan-3-yl ester
• CAS No.: 173033-98-2
• Molecular Formula: C₂₃H₂₇N₅O₆S
• Molecular Weight: 501.563

Synonyms:Benzoic acid (2R,3S,5R)-5-(2-isobutyrylamino-6-oxo-1,6-dihydro-purin-9-yl)-2-methylsulfanylmethoxymethyl-tetrahydro-furan-3-yl ester

Chemical Property of Benzoic acid (2R,3S,5R)-5-(2-isobutyrylamino-6-oxo-1,6-dihydro-purin-9-yl)-2-methylsulfanylmethoxymethyl-tetrahydro-furan-3-yl ester

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Technology Process of Benzoic acid (2R,3S,5R)-5-(2-isobutyrylamino-6-oxo-1,6-dihydro-purin-9-yl)-2-methylsulfanylmethoxymethyl-tetrahydro-furan-3-yl ester

There total 1 articles about Benzoic acid (2R,3S,5R)-5-(2-isobutyrylamino-6-oxo-1,6-dihydro-purin-9-yl)-2-methylsulfanylmethoxymethyl-tetrahydro-furan-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

dimethylsulfide (75-18-3) + 3'-O-benzoyl-N2-isobutyryl-2'-deoxyguanosine (63660-23-1) → Benzoic acid (2R,3S,5R)-5-(2-isobutyrylamino-6-oxo-1,6-dihydro-purin-9-yl)-2-methylsulfanylmethoxymethyl-tetrahydro-furan-3-yl ester (173033-98-2)

Guidance literature:

With dibenzoyl peroxide;

DOI:10.1016/0040-4039(95)01809-V

Reference yield: 70.0%

diphenyl-phosphinic acid (1707-03-5) + Benzoic acid (2R,3S,5R)-5-(2-isobutyrylamino-6-oxo-1,6-dihydro-purin-9-yl)-2-methylsulfanylmethoxymethyl-tetrahydro-furan-3-yl ester (173033-98-2) → Benzoic acid (2R,3S,5R)-2-(diphenyl-phosphinoyloxymethoxymethyl)-5-(2-isobutyrylamino-6-oxo-1,6-dihydro-purin-9-yl)-tetrahydro-furan-3-yl ester (173034-01-0)

Guidance literature:

With N-iodo-succinimide; In diethyl ether; 1,2-dichloro-ethane; Ambient temperature;

DOI:10.1016/0040-4039(95)01809-V

Reference yield: 10.0%

Benzoic acid (2R,3S,5R)-5-(2-isobutyrylamino-6-oxo-1,6-dihydro-purin-9-yl)-2-methylsulfanylmethoxymethyl-tetrahydro-furan-3-yl ester (173033-98-2) → (3R,5S)-1-Benzyl-5-methyl-pyrrolidin-3-ol (152673-19-3) + (3S,5S)-1-Benzyl-5-methyl-pyrrolidin-3-ol

Guidance literature:

With sodium tetrahydroborate; In methanol; for 14h; -78 deg C up to RT;

DOI:10.1016/0040-4039(95)01813-W

upstream raw materials:

dimethylsulfide

3'-O-benzoyl-N²-isobutyryl-2'-deoxyguanosine

Downstream raw materials:

Benzoic acid (2R,3S,5R)-2-(diphenyl-phosphinoyloxymethoxymethyl)-5-(2-isobutyrylamino-6-oxo-1,6-dihydro-purin-9-yl)-tetrahydro-furan-3-yl ester

(3R,5S)-1-Benzyl-5-methyl-pyrrolidin-3-ol

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