S,S-dimethyl N-(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-carbonimidodithioate

Base Information

Chemical Name:S,S-dimethyl N-(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-carbonimidodithioate
CAS No.:221493-37-4
Molecular Formula:C₁₃H₁₉NO₃S₃
Molecular Weight:333.497
Hs Code.:

Synonyms:S,S-dimethyl N-(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-carbonimidodithioate

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Chemical Property of S,S-dimethyl N-(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-carbonimidodithioate

Chemical Property:

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Technology Process of S,S-dimethyl N-(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-carbonimidodithioate

There total 1 articles about S,S-dimethyl N-(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-carbonimidodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 75-15-0,12122-00-8
carbon disulfide

: 316831-31-9
4-methoxy-2,3,6-trimethylbenzenesulfonamide

: 74-88-4
methyl iodide

: 221493-37-4
S,S-dimethyl N-(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-carbonimidodithioate

Guidance literature:: carbon disulfide; 4-methoxy-2,3,6-trimethylbenzenesulfonamide; With potassium hydroxide; In water; N,N-dimethyl-formamide; at 0 ℃; for 0.5h; Inert atmosphere; Cooling with ice;

methyl iodide; In water; N,N-dimethyl-formamide; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/acs.orglett.7b00946

Reference yield: 77.0%

: 162145-93-9
(S)-3-amino-7-methyl-6-octen-1-ol

: 221493-37-4
S,S-dimethyl N-(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-carbonimidodithioate

: 221493-39-6
N-[1-[(S)-1-(2-Hydroxy-ethyl)-5-methyl-hex-4-enylamino]-1-methylsulfanyl-meth-(Z)-ylidene]-4-methoxy-2,3,6-trimethyl-benzenesulfonamide

Guidance literature:: In benzene; for 2h; Heating;
DOI:10.1021/jo981972g

Reference yield:

: 221493-37-4
S,S-dimethyl N-(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-carbonimidodithioate

: (E)-N-{[benzyl(but-3-en-1-yl)amino][benzylamino]methylene}-4-methoxy-2,3,6-trimethylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 2 h / Inert atmosphere; Reflux

2: mercury(II) oxide; triethylamine / ethanol / 72 h / 20 °C / Inert atmosphere

With triethylamine; mercury(II) oxide; In ethanol;
DOI:10.1021/acs.orglett.7b00946