6-{4-[1-benzyl-1H-(1,2,3)-triazole-4-yl]butyl}-3-(2-deoxy-5-O-(4,4'-dimethoxytriphenylmethyl)-β-D-erythropentofuranosyl)pyrrolo[2,3-d]pyrimidin-2(3H)one

Base Information

Chemical Name:6-{4-[1-benzyl-1H-(1,2,3)-triazole-4-yl]butyl}-3-(2-deoxy-5-O-(4,4'-dimethoxytriphenylmethyl)-β-D-erythropentofuranosyl)pyrrolo[2,3-d]pyrimidin-2(3H)one
CAS No.:1402544-65-3
Molecular Formula:C₄₅H₄₆N₆O₆
Molecular Weight:766.897
Hs Code.:

6-{4-[1-benzyl-1H-(1,2,3)-triazole-4-yl]butyl}-3-(2-deoxy-5-O-(4,4'-dimethoxytriphenylmethyl)-β-D-erythropentofuranosyl)pyrrolo[2,3-d]pyrimidin-2(3H)one

Synonyms:6-{4-[1-benzyl-1H-(1,2,3)-triazole-4-yl]butyl}-3-(2-deoxy-5-O-(4,4'-dimethoxytriphenylmethyl)-β-D-erythropentofuranosyl)pyrrolo[2,3-d]pyrimidin-2(3H)one

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Chemical Property of 6-{4-[1-benzyl-1H-(1,2,3)-triazole-4-yl]butyl}-3-(2-deoxy-5-O-(4,4'-dimethoxytriphenylmethyl)-β-D-erythropentofuranosyl)pyrrolo[2,3-d]pyrimidin-2(3H)one

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Technology Process of 6-{4-[1-benzyl-1H-(1,2,3)-triazole-4-yl]butyl}-3-(2-deoxy-5-O-(4,4'-dimethoxytriphenylmethyl)-β-D-erythropentofuranosyl)pyrrolo[2,3-d]pyrimidin-2(3H)one

There total 3 articles about 6-{4-[1-benzyl-1H-(1,2,3)-triazole-4-yl]butyl}-3-(2-deoxy-5-O-(4,4'-dimethoxytriphenylmethyl)-β-D-erythropentofuranosyl)pyrrolo[2,3-d]pyrimidin-2(3H)one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1402544-60-8
6-{4-[1-benzyl-1H-(1,2,3)-triazole-4-yl]butyl}-3-(2-deoxy-β-D-erythropentofuranosyl)pyrrolo[2,3-d]pyrimidin-2(3H)one

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 1402544-65-3
6-{4-[1-benzyl-1H-(1,2,3)-triazole-4-yl]butyl}-3-(2-deoxy-5-O-(4,4'-dimethoxytriphenylmethyl)-β-D-erythropentofuranosyl)pyrrolo[2,3-d]pyrimidin-2(3H)one

Guidance literature:: With pyridine;
DOI:10.1002/chem.201103385

Reference yield:

: 1033295-11-2
3-(2-deoxy-β-D-erythro-pentofuranosyl)-3,7-dihydro-6-hexynyl-2H-pyrrolo[2,3-d]pyrimidin-2-one

: 1402544-65-3
6-{4-[1-benzyl-1H-(1,2,3)-triazole-4-yl]butyl}-3-(2-deoxy-5-O-(4,4'-dimethoxytriphenylmethyl)-β-D-erythropentofuranosyl)pyrrolo[2,3-d]pyrimidin-2(3H)one

Guidance literature:: Multi-step reaction with 2 steps

1: copper(II) sulfate; sodium L-ascorbate; benzoic acid / water; tert-butyl alcohol / 24 h / 20 °C

2: pyridine

With pyridine; copper(II) sulfate; sodium L-ascorbate; benzoic acid; In water; tert-butyl alcohol;
DOI:10.1002/chem.201103385

Reference yield:

: 622-79-7
benzyl azide

: 1402544-65-3
6-{4-[1-benzyl-1H-(1,2,3)-triazole-4-yl]butyl}-3-(2-deoxy-5-O-(4,4'-dimethoxytriphenylmethyl)-β-D-erythropentofuranosyl)pyrrolo[2,3-d]pyrimidin-2(3H)one

Guidance literature:: Multi-step reaction with 2 steps

1: copper(II) sulfate; sodium L-ascorbate; benzoic acid / water; tert-butyl alcohol / 24 h / 20 °C

2: pyridine

With pyridine; copper(II) sulfate; sodium L-ascorbate; benzoic acid; In water; tert-butyl alcohol;
DOI:10.1002/chem.201103385