(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-L-phenylalanine

Base Information

Chemical Name:(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-L-phenylalanine
CAS No.:1412696-84-4
Molecular Formula:C₂₁H₂₈N₄O₇
Molecular Weight:448.476
Hs Code.:

Synonyms:(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-L-phenylalanine

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Chemical Property of (6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-L-phenylalanine

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Technology Process of (6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-L-phenylalanine

There total 3 articles about (6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-L-phenylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1412696-80-0
(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-L-phenylalanine methyl ester

: 1412696-84-4
(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-L-phenylalanine

Guidance literature:: With water; barium(II) hydroxide; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1002/ejoc.201200463

Reference yield:

: 229643-36-1
methyl 6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonate

: 1412696-84-4
(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-L-phenylalanine

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; barium(II) hydroxide / tetrahydrofuran / 3 h / 20 °C

2.1: O-(benzotriazol-1-yl )-N,N,N' ,N'-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 0.08 h

2.2: 20 h / 20 °C / Inert atmosphere

3.1: water; barium(II) hydroxide / tetrahydrofuran / 3 h / 20 °C

With O-(benzotriazol-1-yl )-N,N,N' ,N'-tetramethyluronium tetrafluoroborate; water; barium(II) hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201200463

Reference yield:

: 668990-26-9
6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonic acid

: 1412696-84-4
(6-azido-6-deoxy-2,3:4,5-di-O-isopropylidene-D-galactonyl)-L-phenylalanine

Guidance literature:: Multi-step reaction with 2 steps

1.1: O-(benzotriazol-1-yl )-N,N,N' ,N'-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 0.08 h

1.2: 20 h / 20 °C / Inert atmosphere

2.1: water; barium(II) hydroxide / tetrahydrofuran / 3 h / 20 °C

With O-(benzotriazol-1-yl )-N,N,N' ,N'-tetramethyluronium tetrafluoroborate; water; barium(II) hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201200463