7-(3,5-Di-tert-butylphenyl)-2,12-bis(2-tert-butylacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

Base Information

Chemical Name:7-(3,5-Di-tert-butylphenyl)-2,12-bis(2-tert-butylacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine
CAS No.:111773-21-8
Molecular Formula:C₆₉H₆₇N₃
Molecular Weight:938.311
Hs Code.:

7-(3,5-Di-tert-butylphenyl)-2,12-bis(2-tert-butylacridin-9-yl)-5,6,8,9-tetrahydrodibenz<c,h>acridine

Synonyms:7-(3,5-Di-tert-butylphenyl)-2,12-bis(2-tert-butylacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

Suppliers and Price of 7-(3,5-Di-tert-butylphenyl)-2,12-bis(2-tert-butylacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-(3,5-Di-tert-butylphenyl)-2,12-bis(2-tert-butylacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 7-(3,5-Di-tert-butylphenyl)-2,12-bis(2-tert-butylacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

There total 8 articles about 7-(3,5-Di-tert-butylphenyl)-2,12-bis(2-tert-butylacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 111773-15-0
7-(2-tert-Butylacridin-9-yl)-1-oxo-1,2,3,4-tetrahydronaphthalene

: 111773-18-3
2-(3,5-Di-tert-butylbenzylidene)-7-(2-tert-butylacridin-9-yl)-1-oxo-1,2,3,4-tetrahydronaphthalene

: 111773-21-8
7-(3,5-Di-tert-butylphenyl)-2,12-bis(2-tert-butylacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

Guidance literature:: With perchloric acid; ammonia; 2.) MeOH;
DOI:10.1021/ja00259a055

Reference yield:

: 17610-00-3
3,5-Di-tert-butylbenzaldehyde

: 111773-21-8
7-(3,5-Di-tert-butylphenyl)-2,12-bis(2-tert-butylacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / 4percent KOH / methanol

2: 58 percent / 1.) HClO₄; 2.) NH₃ / 2.) MeOH

With potassium hydroxide; perchloric acid; ammonia; In methanol;
DOI:10.1021/ja00259a055

Reference yield:

: 32281-97-3
7-bromo-3,4-dihydro-2H-naphthalen-1-one

: 111773-21-8
7-(3,5-Di-tert-butylphenyl)-2,12-bis(2-tert-butylacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / p-toluenesulfonic acid / toluene / 12 h / Heating

3: 81 percent / CH₃ONa / methanol / 2.5 h / 70 - 80 °C

4: 1.) 70percent perchloric acid / 1.) 100 deg C, 15 min; 135 deg C, 3 h, 2.) C₂H₅OH, reflux, 5 min

5: NH₃ / methanol; CH₂Cl₂

With perchloric acid; ammonia; sodium methylate; toluene-4-sulfonic acid; In methanol; dichloromethane; toluene;
DOI:10.1021/ja00186a035