(S)-4-((1S,5R,7R)-10,10-Dimethyl-2-oxo-3-phenyl-3,4-diaza-tricyclo[5.2.1.0^1,5]dec-4-yl)-3-hydroxy-2-methylene-4-oxo-butyric acid phenyl ester

Base Information

• Chemical Name: (S)-4-((1S,5R,7R)-10,10-Dimethyl-2-oxo-3-phenyl-3,4-diaza-tricyclo[5.2.1.0^1,5]dec-4-yl)-3-hydroxy-2-methylene-4-oxo-butyric acid phenyl ester
• CAS No.: 682806-85-5
• Molecular Formula: C₂₇H₂₈N₂O₅
• Molecular Weight: 460.53

Synonyms:(S)-4-((1S,5R,7R)-10,10-Dimethyl-2-oxo-3-phenyl-3,4-diaza-tricyclo[5.2.1.0^1,5]dec-4-yl)-3-hydroxy-2-methylene-4-oxo-butyric acid phenyl ester

Chemical Property of (S)-4-((1S,5R,7R)-10,10-Dimethyl-2-oxo-3-phenyl-3,4-diaza-tricyclo[5.2.1.0^1,5]dec-4-yl)-3-hydroxy-2-methylene-4-oxo-butyric acid phenyl ester

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Technology Process of (S)-4-((1S,5R,7R)-10,10-Dimethyl-2-oxo-3-phenyl-3,4-diaza-tricyclo[5.2.1.0^1,5]dec-4-yl)-3-hydroxy-2-methylene-4-oxo-butyric acid phenyl ester

There total 1 articles about (S)-4-((1S,5R,7R)-10,10-Dimethyl-2-oxo-3-phenyl-3,4-diaza-tricyclo[5.2.1.0^1,5]dec-4-yl)-3-hydroxy-2-methylene-4-oxo-butyric acid phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

phenyl acrylate (937-41-7) + (10,10-dimethyl-2-oxo-3-phenyl-3,4-diazatricyclo[5.2.1.01,5]dec-4-yl)-oxoacetaldehyde (682806-82-2) → (S)-4-((1S,5R,7R)-10,10-Dimethyl-2-oxo-3-phenyl-3,4-diaza-tricyclo[5.2.1.01,5]dec-4-yl)-3-hydroxy-2-methylene-4-oxo-butyric acid phenyl ester (682806-85-5)

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; In water; dimethyl sulfoxide; for 1h;

DOI:10.1016/j.tetlet.2004.02.001

Reference yield: 81.0%

N-aminophthalamide (1875-48-5) + (S)-4-((1S,5R,7R)-10,10-Dimethyl-2-oxo-3-phenyl-3,4-diaza-tricyclo[5.2.1.01,5]dec-4-yl)-3-hydroxy-2-methylene-4-oxo-butyric acid phenyl ester (682806-85-5) → (S)-2-[(S)-2-((1S,5R,7R)-10,10-Dimethyl-2-oxo-3-phenyl-3,4-diaza-tricyclo[5.2.1.01,5]dec-4-yl)-1-hydroxy-2-oxo-ethyl]-1-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-aziridine-2-carboxylic acid phenyl ester

Guidance literature:

With lead(IV) acetate;

DOI:10.1016/j.tetlet.2004.02.001

upstream raw materials:

phenyl acrylate

(10,10-dimethyl-2-oxo-3-phenyl-3,4-diazatricyclo[5.2.1.0^1,5]dec-4-yl)-oxoacetaldehyde

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