C₃₉H₄₃N₅O₄

Base Information

Chemical Name:C₃₉H₄₃N₅O₄
CAS No.:1301606-96-1
Molecular Formula:C₃₉H₄₃N₅O₄
Molecular Weight:645.802
Hs Code.:

C<sub>39</sub>H<sub>43</sub>N<sub>5</sub>O<sub>4</sub>

Synonyms:C₃₉H₄₃N₅O₄

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Chemical Property of C₃₉H₄₃N₅O₄

Chemical Property:

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Technology Process of C₃₉H₄₃N₅O₄

There total 7 articles about C₃₉H₄₃N₅O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 512182-37-5
1-(o-methoxybenzyl)-5-phenyl-1H-tetrazole

: 1301606-96-1
C₃₉H₄₃N₅O₄

Guidance literature:: Multi-step reaction with 5 steps

1: 1-methyl-pyrrolidin-2-one; rhodium(III) chloride hydrate; potassium carbonate; triphenylphosphine / 12 h / 140 °C / Inert atmosphere

2: methanol; sodium methylate / 9 h

3: trimethylsilyl bromide / acetonitrile / 4.5 h / 50 °C

4: N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h / 50 °C

5: pyridine / toluene / 9 h / 20 - 40 °C

With pyridine; 1-methyl-pyrrolidin-2-one; methanol; trimethylsilyl bromide; rhodium(III) chloride hydrate; sodium methylate; potassium carbonate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In toluene; acetonitrile;
DOI:10.1021/jo202041e

Reference yield:

: 1301606-99-4
1-((2'-(1-(2-methoxybenzyl)-1H-tetrazol-5-yl)-[1,1'-biphenyl]-4-yl)oxy)propan-2-one

: 1301606-96-1
C₃₉H₄₃N₅O₄

Guidance literature:: Multi-step reaction with 4 steps

1: methanol; sodium methylate / 9 h

2: trimethylsilyl bromide / acetonitrile / 4.5 h / 50 °C

3: N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h / 50 °C

4: pyridine / toluene / 9 h / 20 - 40 °C

With pyridine; methanol; trimethylsilyl bromide; sodium methylate; N-ethyl-N,N-diisopropylamine; In toluene; acetonitrile;
DOI:10.1021/jo202041e

Reference yield:

: 6850-57-3
2-methoxybenzylamine

: 1301606-96-1
C₃₉H₄₃N₅O₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium carbonate / toluene / 0.33 h / 3 - 20 °C

2.1: phosphorus pentachloride / dichloromethane / 2.18 h / -15 - 21 °C

2.2: 4 h / 20 °C

3.1: 1-methyl-pyrrolidin-2-one; rhodium(III) chloride hydrate; potassium carbonate; triphenylphosphine / 12 h / 140 °C / Inert atmosphere

4.1: methanol; sodium methylate / 9 h

5.1: trimethylsilyl bromide / acetonitrile / 4.5 h / 50 °C

6.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h / 50 °C

7.1: pyridine / toluene / 9 h / 20 - 40 °C

With pyridine; 1-methyl-pyrrolidin-2-one; methanol; trimethylsilyl bromide; rhodium(III) chloride hydrate; phosphorus pentachloride; sodium methylate; sodium carbonate; potassium carbonate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In dichloromethane; toluene; acetonitrile;
DOI:10.1021/jo202041e