1-[3-(methylsulfanyl)-2-thienyl]ethanone O-{4-nitrobenzoyl}oxime

Base Information

• Chemical Name: 1-[3-(methylsulfanyl)-2-thienyl]ethanone O-{4-nitrobenzoyl}oxime
• CAS No.: 74598-25-7
• Molecular Formula: C₁₄H₁₂N₂O₄S₂
• Molecular Weight: 336.392
• Mol file: 74598-25-7.mol

Synonyms:(E)-methyl (3-methylthio-2-thienyl) O-p-nitrobenzoylketoxime

Chemical Property of 1-[3-(methylsulfanyl)-2-thienyl]ethanone O-{4-nitrobenzoyl}oxime

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1-[3-(methylsulfanyl)-2-thienyl]ethanone O-{4-nitrobenzoyl}oxime

There total 1 articles about 1-[3-(methylsulfanyl)-2-thienyl]ethanone O-{4-nitrobenzoyl}oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

4-nitro-benzoyl chloride (122-04-3) + (E)-2-acetyl-3-methylthiothiophen oxime (74598-26-8) → (E)-methyl (3-methylthio-2-thienyl) O-p-nitrobenzoylketoxime (74598-25-7)

Guidance literature:

With sodium hydride; In diethyl ether; N,N-dimethyl-formamide;

Reference yield: 37.0%

(E)-methyl (3-methylthio-2-thienyl) O-p-nitrobenzoylketoxime (74598-25-7) → methyl-2 thieno<2,3-d>thiazole (61612-02-0)

Guidance literature:

With sulfuric acid; for 3h; Ambient temperature;

upstream raw materials:

4-nitro-benzoyl chloride

(E)-2-acetyl-3-methylthiothiophen oxime

Downstream raw materials:

methyl-2 thieno<2,3-d>thiazole