C₂₉H₃₆N₂O₅

Base Information

Chemical Name:C₂₉H₃₆N₂O₅
CAS No.:1599423-23-0
Molecular Formula:C₂₉H₃₆N₂O₅
Molecular Weight:492.615
Hs Code.:

C<sub>29</sub>H<sub>36</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₉H₃₆N₂O₅

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Chemical Property of C₂₉H₃₆N₂O₅

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Technology Process of C₂₉H₃₆N₂O₅

There total 6 articles about C₂₉H₃₆N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1469-70-1
allyl ethyl carbonate

: 1599423-21-8
N-(tert-butyloxycarbonyl)sarcosine {N-[4-benzoyloxy-(2E)-buten-1-yl]-N-benzyl}amide

: 1599423-23-0
C₂₉H₃₆N₂O₅

Guidance literature:: N-(tert-butyloxycarbonyl)sarcosine {N-[4-benzoyloxy-(2E)-buten-1-yl]-N-benzyl}amide; With n-butyllithium; 1,1,1,3,3,3-hexamethyl-disilazane; zinc(II) chloride; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Schlenk technique; Inert atmosphere;

allyl ethyl carbonate; With bis(η3-allyl-μ-chloropalladium(II)); triphenylphosphine; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 16h; Schlenk technique; Inert atmosphere;
DOI:10.1002/ejoc.201301659

Reference yield:

: 1599423-01-4
N-(tert-butyloxycarbonyl)sarcosine {N-benzyl-N-[4-tert-butyldimethylsilyloxy-(2E)-buten-1-yl]}amide

: 1599423-23-0
C₂₉H₃₆N₂O₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h

2.1: pyridine; dmap / dichloromethane / 0 - 20 °C / Inert atmosphere

3.1: n-butyllithium; 1,1,1,3,3,3-hexamethyl-disilazane; zinc(II) chloride / tetrahydrofuran; hexane / 0.5 h / -78 °C / Schlenk technique; Inert atmosphere

3.2: 16 h / -78 - 20 °C / Schlenk technique; Inert atmosphere

With pyridine; dmap; n-butyllithium; tetrabutyl ammonium fluoride; 1,1,1,3,3,3-hexamethyl-disilazane; zinc(II) chloride; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1002/ejoc.201301659

Reference yield:

: 1099751-95-7
(2E)-N-benzyl-4-(tert-butyldimethylsiloxy)but-2-en-1-amine

: 1599423-23-0
C₂₉H₃₆N₂O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-ethyl-N,N-diisopropylamine; 2-bromo-1-ethylpyridin-1-ium tetrafluoroborate / dichloromethane / -10 - 20 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h

3.1: pyridine; dmap / dichloromethane / 0 - 20 °C / Inert atmosphere

4.1: n-butyllithium; 1,1,1,3,3,3-hexamethyl-disilazane; zinc(II) chloride / tetrahydrofuran; hexane / 0.5 h / -78 °C / Schlenk technique; Inert atmosphere

4.2: 16 h / -78 - 20 °C / Schlenk technique; Inert atmosphere

With pyridine; dmap; n-butyllithium; tetrabutyl ammonium fluoride; 2-bromo-1-ethylpyridin-1-ium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; 1,1,1,3,3,3-hexamethyl-disilazane; zinc(II) chloride; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1002/ejoc.201301659