C₃₆H₅₈N₄O₉SSi

Base Information

Chemical Name:C₃₆H₅₈N₄O₉SSi
CAS No.:1300656-00-1
Molecular Formula:C₃₆H₅₈N₄O₉SSi
Molecular Weight:751.029
Hs Code.:

C<sub>36</sub>H<sub>58</sub>N<sub>4</sub>O<sub>9</sub>SSi

Synonyms:C₃₆H₅₈N₄O₉SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₆H₅₈N₄O₉SSi

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Technology Process of C₃₆H₅₈N₄O₉SSi

There total 19 articles about C₃₆H₅₈N₄O₉SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1300655-99-5
C₃₆H₅₈N₄O₇SSi

: 1300656-00-1
C₃₆H₅₈N₄O₉SSi

Guidance literature:: With ammonium heptamolybdate tetrahydrate; dihydrogen peroxide; In ethanol; water; for 12h; Inert atmosphere;
DOI:10.1021/ja201467z

Reference yield:

: 1300655-86-0
C₁₃H₁₈O₂

: 1300656-00-1
C₃₆H₅₈N₄O₉SSi

Guidance literature:: Multi-step reaction with 16 steps

1.1: n-butyllithium / hexane; tert-butyl methyl ether / 0.17 h / -78 °C / Inert atmosphere

1.2: 0.67 h / 0 - 20 °C / Inert atmosphere

2.1: sodium hydride / hexane / 2 h / Inert atmosphere; Reflux

3.1: acetylacetonatodicarbonylrhodium(l) / benzene / 4.5 h / 60 °C / 51716.2 Torr / Autoclave

3.2: 1 h / 40 °C / Inert atmosphere

4.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere

5.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

5.2: -78 - 20 °C / Inert atmosphere

6.1: toluene / 18 h / Inert atmosphere; Reflux

7.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide; citric acid / tetrahydrofuran; tert-butyl alcohol / 24 h / Inert atmosphere

8.1: sodium periodate; sodium hydrogencarbonate / tetrahydrofuran; water / 1 h / 0 °C / Inert atmosphere

9.1: tetra-(n-butyl)ammonium iodide / dichloromethane; water / 3 h / Inert atmosphere

10.1: acetylacetonatodicarbonylrhodium(l); hydrogen; triphenylphosphine / tetrahydrofuran / 24 h / 20 - 50 °C / 25858.1 Torr / Autoclave

11.1: pyridine; dmap / dichloromethane / 16 h / -20 °C / Inert atmosphere

12.1: titanium tetrachloride / dichloromethane / 0.08 h / 0 °C / Inert atmosphere

12.2: 3 h / -40 °C / Inert atmosphere

13.1: dmap / 24 h / Inert atmosphere

14.1: 5% Pd(II)/C(eggshell); hydrogen / tetrahydrofuran / 2 h / 760.05 Torr

15.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 24 h / Inert atmosphere

16.1: ammonium heptamolybdate tetrahydrate; dihydrogen peroxide / ethanol; water / 12 h / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; dmap; acetylacetonatodicarbonylrhodium(l); sodium periodate; osmium(VIII) oxide; n-butyllithium; ammonium heptamolybdate tetrahydrate; di-isopropyl azodicarboxylate; 5% Pd(II)/C(eggshell); water; hydrogen; dihydrogen peroxide; titanium tetrachloride; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; 4-methylmorpholine N-oxide; triphenylphosphine; citric acid; In tetrahydrofuran; ethanol; hexane; dichloromethane; tert-butyl methyl ether; water; toluene; tert-butyl alcohol; benzene; 9.1: Felkin addition;
DOI:10.1021/ja201467z

Reference yield:

: 1300655-98-4
C₂₉H₅₄O₈Si

: 1300656-00-1
C₃₆H₅₈N₄O₉SSi

Guidance literature:: Multi-step reaction with 2 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 24 h / Inert atmosphere

2: ammonium heptamolybdate tetrahydrate; dihydrogen peroxide / ethanol; water / 12 h / Inert atmosphere

With ammonium heptamolybdate tetrahydrate; di-isopropyl azodicarboxylate; dihydrogen peroxide; triphenylphosphine; In tetrahydrofuran; ethanol; water;
DOI:10.1021/ja201467z