C₆H₁₀O₄(C₃H₄)2(C₇H₆)O₂H₂PO(OC₇H₆)2H

Base Information

• Chemical Name: C₆H₁₀O₄(C₃H₄)2(C₇H₆)O₂H₂PO(OC₇H₆)2H
• CAS No.: 956117-03-6
• Molecular Formula: C₃₃H₃₉O₉P
• Molecular Weight: 610.641
• Mol file: 956117-03-6.mol

Synonyms:C₆H₁₀O₄(C₃H₄)2(C₇H₆)O₂H₂PO(OC₇H₆)2H

Chemical Property of C₆H₁₀O₄(C₃H₄)2(C₇H₆)O₂H₂PO(OC₇H₆)2H

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆H₁₀O₄(C₃H₄)2(C₇H₆)O₂H₂PO(OC₇H₆)2H

There total 8 articles about C₆H₁₀O₄(C₃H₄)2(C₇H₆)O₂H₂PO(OC₇H₆)2H which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C6H10O4(C3H4)2(C7H6)O2H2P(OC7H6)2H → C6H10O4(C3H4)2(C7H6)O2H2PO(OC7H6)2H (956117-03-6)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide; at 0 - 20 ℃;

DOI:10.1080/07328300701540225

Reference yield:

benzyl bromide (100-39-0) → C6H10O4(C3H4)2(C7H6)O2H2PO(OC7H6)2H (956117-03-6)

Guidance literature:

Multi-step reaction with 6 steps

1: NaH; TBAI / tetrahydrofuran / 0 - 20 °C

2: NMO / OsO₄ / acetone; H₂O / 12 h / 20 °C

3: TSA / CH₂Cl₂ / 1 h / 20 °C

4: H₂; NaHCO₃ / Pd/C / tetrahydrofuran / 72 h / 20 °C / 760.05 Torr

5: 1H-tetrazole / dimethylformamide; CH₂Cl₂ / 7 h / 20 °C

6: m-CPBA / dimethylformamide; CH₂Cl₂ / 0 - 20 °C

With 1H-tetrazole; N-methyl-2-indolinone; hydrogen; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; osmium(VIII) oxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetone;

DOI:10.1080/07328300701540225

Reference yield:

(3aS,4S,4aR,7aS,8S,8aS)-4,8-Bis-benzyloxy-2,2,6,6-tetramethyl-hexahydro-benzo[1,2-d;4,5-d']bis[1,3]dioxole (160636-42-0) → C6H10O4(C3H4)2(C7H6)O2H2PO(OC7H6)2H (956117-03-6)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂; NaHCO₃ / Pd/C / tetrahydrofuran / 72 h / 20 °C / 760.05 Torr

2: 1H-tetrazole / dimethylformamide; CH₂Cl₂ / 7 h / 20 °C

3: m-CPBA / dimethylformamide; CH₂Cl₂ / 0 - 20 °C

With 1H-tetrazole; hydrogen; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1080/07328300701540225

upstream raw materials:

Dibenzyl N,N-diisopropylphosphoramidite

benzyl bromide

1D-4-O-benzyl-2,3:5,6-di-O-isopropylidene-myo-inositol

(3aS,4S,4aR,7aS,8S,8aS)-4,8-Bis-benzyloxy-2,2,6,6-tetramethyl-hexahydro-benzo[1,2-d;4,5-d']bis[1,3]dioxole

Downstream raw materials:

myo-inositol 1-phosphate

Refernces