C₃₈H₃₉BN₂O₈

Base Information

Chemical Name:C₃₈H₃₉BN₂O₈
CAS No.:1425051-97-3
Molecular Formula:C₃₈H₃₉BN₂O₈
Molecular Weight:662.547
Hs Code.:

C<sub>38</sub>H<sub>39</sub>BN<sub>2</sub>O<sub>8</sub>

Synonyms:C₃₈H₃₉BN₂O₈

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Chemical Property of C₃₈H₃₉BN₂O₈

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Technology Process of C₃₈H₃₉BN₂O₈

There total 12 articles about C₃₈H₃₉BN₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1425052-09-0
C₄₄H₅₃BN₂O₈Si

: 1425051-97-3
C₃₈H₃₉BN₂O₈

Guidance literature:: C₄₄H₅₃BN₂O₈Si; With toluene-4-sulfonic acid; In tetrahydrofuran; water; at 23 ℃; for 14h; Inert atmosphere;

With 2,3-dimethyl-2,3-butane diol; triethylamine; In tetrahydrofuran; water; at 23 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jo400105m

Reference yield:

: 1425052-06-7
C₁₈H₂₄O₂Si

: 1425051-97-3
C₃₈H₃₉BN₂O₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: toluene-4-sulfonic acid / tetrahydrofuran; water / 14 h / 23 °C / Inert atmosphere

2.1: diphenylphosphoranyl azide; triethylamine / benzene / 1 h / 85 °C / Inert atmosphere

2.2: 3 h / 85 °C / Inert atmosphere

3.1: sodium dihydrogen phosphate monohydrate; sodium chlorite; 2-methyl-but-2-ene / water; acetone / 0.5 h / 23 °C / Inert atmosphere

4.1: diphenylphosphoranyl azide; triethylamine / benzene / 1 h / 85 °C / Inert atmosphere

4.2: 3 h / 85 °C / Inert atmosphere

5.1: toluene-4-sulfonic acid / tetrahydrofuran; water / 14 h / 23 °C / Inert atmosphere

5.2: 24 h / 23 °C / Inert atmosphere

With sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; diphenylphosphoranyl azide; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; water; acetone; benzene; 2.1: |Curtius Rearrangement / 2.2: |Curtius Rearrangement / 4.1: |Curtius Rearrangement / 4.2: |Curtius Rearrangement;
DOI:10.1021/jo400105m

Reference yield:

: 79996-99-9
1-bromo-4-bromomethyl-naphthalene

: 1425051-97-3
C₃₈H₃₉BN₂O₈

Guidance literature:: Multi-step reaction with 8 steps

1.1: calcium carbonate / water; 1,4-dioxane / 12 h / 110 °C / Inert atmosphere

2.1: dmap; 1H-imidazole / dichloromethane / 16 h / 23 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.08 h / -78 °C / Inert atmosphere

3.2: 1.5 h / -78 - 23 °C / Inert atmosphere

4.1: toluene-4-sulfonic acid / tetrahydrofuran; water / 14 h / 23 °C / Inert atmosphere

5.1: diphenylphosphoranyl azide; triethylamine / benzene / 1 h / 85 °C / Inert atmosphere

5.2: 3 h / 85 °C / Inert atmosphere

6.1: sodium dihydrogen phosphate monohydrate; sodium chlorite; 2-methyl-but-2-ene / water; acetone / 0.5 h / 23 °C / Inert atmosphere

7.1: diphenylphosphoranyl azide; triethylamine / benzene / 1 h / 85 °C / Inert atmosphere

7.2: 3 h / 85 °C / Inert atmosphere

8.1: toluene-4-sulfonic acid / tetrahydrofuran; water / 14 h / 23 °C / Inert atmosphere

8.2: 24 h / 23 °C / Inert atmosphere

With 1H-imidazole; dmap; sodium chlorite; n-butyllithium; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; diphenylphosphoranyl azide; toluene-4-sulfonic acid; triethylamine; calcium carbonate; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; water; acetone; benzene; 5.1: |Curtius Rearrangement / 5.2: |Curtius Rearrangement / 7.1: |Curtius Rearrangement / 7.2: |Curtius Rearrangement;
DOI:10.1021/jo400105m