(2R,5S)-5-benzyl-(t-butoxycarbonylamino)-3-methyl-2-(1-phenylvinyl)-2,3-dihydroimidazolidin-4(5H)-one

Base Information

• Chemical Name: (2R,5S)-5-benzyl-(t-butoxycarbonylamino)-3-methyl-2-(1-phenylvinyl)-2,3-dihydroimidazolidin-4(5H)-one
• CAS No.: 1133721-64-8
• Molecular Formula: C₂₄H₂₈N₂O₃
• Molecular Weight: 392.498

Synonyms:(2R,5S)-5-benzyl-(t-butoxycarbonylamino)-3-methyl-2-(1-phenylvinyl)-2,3-dihydroimidazolidin-4(5H)-one

Chemical Property of (2R,5S)-5-benzyl-(t-butoxycarbonylamino)-3-methyl-2-(1-phenylvinyl)-2,3-dihydroimidazolidin-4(5H)-one

Chemical Property:

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Technology Process of (2R,5S)-5-benzyl-(t-butoxycarbonylamino)-3-methyl-2-(1-phenylvinyl)-2,3-dihydroimidazolidin-4(5H)-one

There total 1 articles about (2R,5S)-5-benzyl-(t-butoxycarbonylamino)-3-methyl-2-(1-phenylvinyl)-2,3-dihydroimidazolidin-4(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

iodobenzene (591-50-4) + (S)-2-(t-butoxycarbonylamino)-N-methyl-3-phenyl-N-(1,2-propadienyl)propanamide (1133721-59-1) → (2S,5S)-5-benzyl-(t-butoxycarbonylamino)-3-methyl-2-(1-phenylvinyl)-2,3-dihydroimidazolidin-4(5H)-one (1133721-69-3) + (2R,5S)-5-benzyl-(t-butoxycarbonylamino)-3-methyl-2-(1-phenylvinyl)-2,3-dihydroimidazolidin-4(5H)-one (1133721-64-8)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 2h;

DOI:10.1021/ol900171g

Reference yield: 93.0%

(2R,5S)-5-benzyl-(t-butoxycarbonylamino)-3-methyl-2-(1-phenylvinyl)-2,3-dihydroimidazolidin-4(5H)-one (1133721-64-8) → (2S,5S)-5-benzyl-3-methyl-2-(1-phenylvinyl)imidazolidin-4-one (1225031-32-2)

Guidance literature:

With trifluoroacetic acid; at 20 ℃; for 3h;

DOI:10.1002/ejoc.200901290

upstream raw materials:

iodobenzene

(S)-2-(t-butoxycarbonylamino)-N-methyl-3-phenyl-N-(1,2-propadienyl)propanamide

Downstream raw materials:

(2S,5S)-5-benzyl-3-methyl-2-(1-phenylvinyl)imidazolidin-4-one

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