(Z),(R)-N-but-3-enyl-N-(1-cyclohexyl-penta-2,4-dienyl)-4-methyl-benzensulfonamide

Base Information

Chemical Name:(Z),(R)-N-but-3-enyl-N-(1-cyclohexyl-penta-2,4-dienyl)-4-methyl-benzensulfonamide
CAS No.:944131-48-0
Molecular Formula:C₂₂H₃₁NO₂S
Molecular Weight:373.56
Hs Code.:

Synonyms:(Z),(R)-N-but-3-enyl-N-(1-cyclohexyl-penta-2,4-dienyl)-4-methyl-benzensulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z),(R)-N-but-3-enyl-N-(1-cyclohexyl-penta-2,4-dienyl)-4-methyl-benzensulfonamide

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Technology Process of (Z),(R)-N-but-3-enyl-N-(1-cyclohexyl-penta-2,4-dienyl)-4-methyl-benzensulfonamide

There total 2 articles about (Z),(R)-N-but-3-enyl-N-(1-cyclohexyl-penta-2,4-dienyl)-4-methyl-benzensulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 260975-29-9
(E)-N-cyclohexylmethylene-4-toluenesulfonamide

: 944131-48-0
(Z),(R)-N-but-3-enyl-N-(1-cyclohexyl-penta-2,4-dienyl)-4-methyl-benzensulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: H₂; m-nitrobenzoic acid; Na₂SO₄ / [Rh(cod)2]BARF; (S)-Cl,MeO-BIPHEP / toluene / 24 h / 20 °C / 760.05 Torr

2: Cs₂CO₃ / dimethylformamide / 70 °C

With hydrogen; caesium carbonate; sodium sulfate; 3-nitrobenzoic acid; [Rh(COD)2]BARF; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja0715896

Reference yield:

: 5162-44-7
1-bromo-4-butene

: 944131-43-5
(Z),(R)-N-(1-cyclohexyl-penta-2,4-dienyl)-4-methyl-benzensulfonamide

: 944131-48-0
(Z),(R)-N-but-3-enyl-N-(1-cyclohexyl-penta-2,4-dienyl)-4-methyl-benzensulfonamide

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 70 ℃;
DOI:10.1021/ja0715896

Reference yield:

: 944131-48-0
(Z),(R)-N-but-3-enyl-N-(1-cyclohexyl-penta-2,4-dienyl)-4-methyl-benzensulfonamide

: (R)-6-cyclohexyl-1-(toluene-4-sulfonyl)-1,2,3,6-tetrahydro-pyridine

Guidance literature:: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; Heating;
DOI:10.1021/ja0715896