C₁₆H₂₄OSi

Base Information

Chemical Name:C₁₆H₂₄OSi
CAS No.:252949-41-0
Molecular Formula:C₁₆H₂₄OSi
Molecular Weight:260.451
Hs Code.:

Synonyms:C₁₆H₂₄OSi

Suppliers and Price of C₁₆H₂₄OSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₂₄OSi

Chemical Property:

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Technology Process of C₁₆H₂₄OSi

There total 4 articles about C₁₆H₂₄OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1423043-19-9
1-(4-((tert-butyldimethylsilyl)oxy)phenyl)but-3-yn-1-ol

: 252949-41-0
C₁₆H₂₄OSi

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c3ob27491h

Reference yield:

: 120743-99-9
p-[(tert-butyldimethylsilyl)oxy]benzaldehyde

: 252949-41-0
C₁₆H₂₄OSi

Guidance literature:: Multi-step reaction with 2 steps

1.1: zinc; titanium tetrachloride / tetrahydrofuran; toluene / 0.5 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 °C / Inert atmosphere

2.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 4 h / 0 °C / Inert atmosphere

With triethylsilane; boron trifluoride diethyl etherate; titanium tetrachloride; zinc; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ol4006954

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 252949-41-0
C₁₆H₂₄OSi

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap; 1H-imidazole / dichloromethane / 24 h / 20 °C / Inert atmosphere

2.1: zinc; titanium tetrachloride / tetrahydrofuran; toluene / 0.5 h / 0 °C / Inert atmosphere

2.2: 2 h / 0 °C / Inert atmosphere

3.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 4 h / 0 °C / Inert atmosphere

With 1H-imidazole; triethylsilane; dmap; boron trifluoride diethyl etherate; titanium tetrachloride; zinc; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ol4006954