Isoquinolin-1-yl-phenyl-methanol; hydrochloride

Base Information

Chemical Name:Isoquinolin-1-yl-phenyl-methanol; hydrochloride
CAS No.:121451-81-8
Molecular Formula:C₁₆H₁₃NO*ClH
Molecular Weight:271.746
Hs Code.:

Synonyms:Isoquinolin-1-yl-phenyl-methanol; hydrochloride

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Chemical Property of Isoquinolin-1-yl-phenyl-methanol; hydrochloride

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Technology Process of Isoquinolin-1-yl-phenyl-methanol; hydrochloride

There total 3 articles about Isoquinolin-1-yl-phenyl-methanol; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 5468-02-0
benzoyloxy-isoquinolin-1-yl-phenyl-methane

: 121451-81-8
Isoquinolin-1-yl-phenyl-methanol; hydrochloride

Guidance literature:: With hydrogenchloride; potassium hydroxide; In ethanol; dichloromethane; for 1h; ultrasound sonication;

Reference yield:

: 119-65-3
isoquinoline

: 121451-81-8
Isoquinolin-1-yl-phenyl-methanol; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / triethylbenzylammonmium chloride / CH₂Cl₂; H₂O / 0.33 h / Irradiation; ultrasound sonication

2: 1.) 50percent aq. NaOH; 2.) 50percent aq. NaOH; HCl(g) / triethylbenzylammonium chloride / 1.) dichloromethane, 5 min, ultrasound sonication; 2.) dichloromethane, ethanol, 85 min, ultrasound sonication

With hydrogenchloride; sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; water;

Reference yield:

: 844-25-7,55839-33-3
2-benzoyl-1-cyano-1,2-dihydroisoquinoline

: 100-52-7
benzaldehyde

: 121451-81-8
Isoquinolin-1-yl-phenyl-methanol; hydrochloride

Guidance literature:: With hydrogenchloride; sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; Yield given. Multistep reaction; 1.) dichloromethane, 5 min, ultrasound sonication; 2.) dichloromethane, ethanol, 85 min, ultrasound sonication;