Technology Process of C29H48O6
There total 7 articles about C29H48O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetramethylammonium triacetoxyborohydride;
In
acetic acid; acetonitrile;
at -20 - 25 ℃;
for 4h;
DOI:10.1021/ol201426c
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triethylamine; (-)-diisopinocamphenylborane chloride / diethyl ether / 1 h / 0 °C
1.2: 18 h / -78 - -20 °C
2.1: tetramethylammonium triacetoxyborohydride / acetic acid; acetonitrile / 4 h / -20 - 25 °C
With
triethylamine; (-)-diisopinocamphenylborane chloride; tetramethylammonium triacetoxyborohydride;
In
diethyl ether; acetic acid; acetonitrile;
1.2: Aldol condensation;
DOI:10.1021/ol201426c
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: Hoveyda-Grubbs catalyst second generation / toluene / 18 h / 25 °C / Reflux
2.1: triethylamine; (-)-diisopinocamphenylborane chloride / diethyl ether / 1 h / 0 °C
2.2: 18 h / -78 - -20 °C
3.1: tetramethylammonium triacetoxyborohydride / acetic acid; acetonitrile / 4 h / -20 - 25 °C
With
Hoveyda-Grubbs catalyst second generation; triethylamine; (-)-diisopinocamphenylborane chloride; tetramethylammonium triacetoxyborohydride;
In
diethyl ether; acetic acid; toluene; acetonitrile;
2.2: Aldol condensation;
DOI:10.1021/ol201426c