methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate)

Base Information

• Chemical Name: methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate)
• CAS No.: 1091627-02-9
• Molecular Formula: C₂₉H₃₁NO₉S
• Molecular Weight: 569.632

Synonyms:methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate)

Chemical Property of methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate)

Chemical Property:

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Technology Process of methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate)

There total 2 articles about methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-ulopyranosidonate (1091627-01-8) → methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate) (1091627-02-9)

Guidance literature:

With Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/jo801946y

Reference yield: 60.0%

methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate) 1',1'-diphenyl-5-methoxysalicylic alcohol acetal (1091627-03-0) → methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate) (1091627-02-9)

Guidance literature:

In acetonitrile; at 20 ℃; for 1.33333h; Irradiation;

DOI:10.1021/jo801946y

Reference yield: 83.0%

α,α-diphenyl-5-methoxysalicyl alcohol (936716-83-5) + methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate) (1091627-02-9) → methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate) 1',1'-diphenyl-5-methoxysalicylic alcohol acetal (1091627-03-0)

Guidance literature:

With toluene-4-sulfonic acid; In benzene; at 20 ℃; for 24h;

DOI:10.1021/jo801946y

upstream raw materials:

methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-ulopyranosidonate

methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate) 1',1'-diphenyl-5-methoxysalicylic alcohol acetal

Downstream raw materials:

methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate) 1',1'-diphenyl-5-methoxysalicylic alcohol acetal

C₇₂H₇₄N₂O₂₀S

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