methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate) 1',1'-diphenyl-5-methoxysalicylic alcohol acetal

Base Information

• Chemical Name: methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate) 1',1'-diphenyl-5-methoxysalicylic alcohol acetal
• CAS No.: 1091627-03-0
• Molecular Formula: C₄₉H₄₇NO₁₁S
• Molecular Weight: 857.978

Synonyms:methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate) 1',1'-diphenyl-5-methoxysalicylic alcohol acetal

Chemical Property of methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate) 1',1'-diphenyl-5-methoxysalicylic alcohol acetal

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Technology Process of methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate) 1',1'-diphenyl-5-methoxysalicylic alcohol acetal

There total 1 articles about methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate) 1',1'-diphenyl-5-methoxysalicylic alcohol acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

α,α-diphenyl-5-methoxysalicyl alcohol (936716-83-5) + methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate) (1091627-02-9) → methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate) 1',1'-diphenyl-5-methoxysalicylic alcohol acetal (1091627-03-0)

Guidance literature:

With toluene-4-sulfonic acid; In benzene; at 20 ℃; for 24h;

DOI:10.1021/jo801946y

Reference yield: 85.0%

methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate) 1',1'-diphenyl-5-methoxysalicylic alcohol acetal (1091627-03-0) → methyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-phenylsulfonyl-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate) 1',1'-diphenyl-5-methoxysalicylic alcohol acetal (1091627-04-1)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/jo801946y

Reference yield: 60.0%

methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate) 1',1'-diphenyl-5-methoxysalicylic alcohol acetal (1091627-03-0) → methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate) (1091627-02-9)

Guidance literature:

In acetonitrile; at 20 ℃; for 1.33333h; Irradiation;

DOI:10.1021/jo801946y

upstream raw materials:

α,α-diphenyl-5-methoxysalicyl alcohol

methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate)

Downstream raw materials:

methyl phenyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-thio-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate)

methyl 5-(N-acetylacetamido)-3,5-dideoxy-4,7,8-tri-O-propargyl-2-phenylsulfonyl-D-glycero-α-D-galacto-non-2-(9-oxaulopyranosidonate) 1',1'-diphenyl-5-methoxysalicylic alcohol acetal

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