Cu₂(C₆H₄(CH₂N(CH₂CH₂C₅H₄N)2)2)⁽²⁺⁾*2PF₆^(1-)=[Cu₂(C₆H₄(CH₂N(CH₂CH₂C₅H₄N)2)2)](PF₆)2

Base Information

• Chemical Name: Cu₂(C₆H₄(CH₂N(CH₂CH₂C₅H₄N)2)2)⁽²⁺⁾*2PF₆^(1-)=[Cu₂(C₆H₄(CH₂N(CH₂CH₂C₅H₄N)2)2)](PF₆)2
• CAS No.: 82731-39-3
• Molecular Formula: C₃₆H₄₀Cu₂N₆*2F₆P
• Molecular Weight: 973.774

Synonyms:Cu₂(C₆H₄(CH₂N(CH₂CH₂C₅H₄N)2)2)⁽²⁺⁾*2PF₆^(1-)=[Cu₂(C₆H₄(CH₂N(CH₂CH₂C₅H₄N)2)2)](PF₆)2

Chemical Property of Cu₂(C₆H₄(CH₂N(CH₂CH₂C₅H₄N)2)2)⁽²⁺⁾*2PF₆^(1-)=[Cu₂(C₆H₄(CH₂N(CH₂CH₂C₅H₄N)2)2)](PF₆)2

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Technology Process of Cu₂(C₆H₄(CH₂N(CH₂CH₂C₅H₄N)2)2)⁽²⁺⁾*2PF₆^(1-)=[Cu₂(C₆H₄(CH₂N(CH₂CH₂C₅H₄N)2)2)](PF₆)2

There total 1 articles about Cu₂(C₆H₄(CH₂N(CH₂CH₂C₅H₄N)2)2)⁽²⁺⁾*2PF₆^(1-)=[Cu₂(C₆H₄(CH₂N(CH₂CH₂C₅H₄N)2)2)](PF₆)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

tetrakis(actonitrile)copper(I) hexafluorophosphate (64443-05-6) + N,N,N',N'-tetrakis{2-(2-pyridyl)ethy}-α,α'-diamino-m-xylene (79854-06-1) → Cu2(C6H4(CH2N(CH2CH2C5H4N)2)2)(2+)*2PF6(1-)=[Cu2(C6H4(CH2N(CH2CH2C5H4N)2)2)](PF6)2 (82731-39-3)

Guidance literature:

In tetrahydrofuran; (Ar); to stirred suspn. of Cu complex was added dropwise ligand, stirring was continued overnight; formed ppt. was filtered off, washed with acetone/ether (1/2), then ether and dried in vac.; elem. anal.;

DOI:10.1021/ja00319a036

Reference yield:

Cu2(C6H4(CH2N(CH2CH2C5H4N)2)2)(2+)*2PF6(1-)=[Cu2(C6H4(CH2N(CH2CH2C5H4N)2)2)](PF6)2 (82731-39-3) + sodium tetraphenyl borate (143-66-8) → {CuO(C6H3(CH2)2)(OCH3)Cu(N(CH2CH2C5H4N)2)2}(2+)*2{B(C6H5)4}(1-)

Guidance literature:

With methanol; O₂; In methanol; dichloromethane; exposing the Cu complex in CH2Cl2 to dry O2, stirring (2 h), concg., washing (CH2Cl2) to yield a soln. and a blue-green ppt., dissolving the ppt. in CH3OH, filtration, pptg. (excess Et2O), redissolving (CH3OH), addn. of Na(BPh4) in CH3OH (all under Ar); immediate color change to light yellow, exposing to O2 to yield a green soln., addn. of Et2O, pptn.;

upstream raw materials:

tetrakis(actonitrile)copper(I) hexafluorophosphate

N,N,N',N'-tetrakis{2-(2-pyridyl)ethy}-α,α'-diamino-m-xylene

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