triphenylamine boronic acid

Base Information

Chemical Name:triphenylamine boronic acid
CAS No.:1172087-54-5
Molecular Formula:C₁₈H₁₆BO₂P
Molecular Weight:306.109
Hs Code.:

Synonyms:triphenylamine boronic acid

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Chemical Property of triphenylamine boronic acid

Chemical Property:

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Technology Process of triphenylamine boronic acid

There total 1 articles about triphenylamine boronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121-43-7,63156-11-6
Trimethyl borate

: 7732-18-5
water

: 734-59-8
(4-bromophenyl)diphenylphosphane

: 1172087-54-5
triphenylamine boronic acid

Guidance literature:: With n-butyllithium; In tetrahydrofuran; byproducts: LiBr; (inert atm., glovebox) THF was condensed to phosphine at -78°C, n-butyllithium was added dropwise, stirred for 2 h, B(OCH3)3 was added, allowed to warm to ambient temp. over 30 min, stirred overnight, H2O was added; diethyl ether was added, the aq. layer was extd. with diethyl ether, theorganic layer was dried over MgSO4, the solvent was removed, dried und er high vac.;
DOI:10.1021/om2004095

Reference yield: 57.0%

: 1172087-54-5
triphenylamine boronic acid

: 3,6-bis(5-bromo-4-decylthiophen-2-yl)-s-tetrazine

: 4-(5-(6-(5-bromo-4-decylthiophen-2-yl)-s-tetrazin-3-yl)-3-decylthiophen-2-yl)-N,N-diphenylaniline

: 4,4'-(5,5'-(s-tetrazine-3,6-diyl)bis(3-decylthiophene-5,2-diyl))bis-(N,N-diphenylaniline)

Guidance literature:: With sodium carbonate; In methanol; water; toluene; at 80 ℃; for 48h; Inert atmosphere;
DOI:10.1039/c5tc00531k

Reference yield:

: 1172087-54-5
triphenylamine boronic acid

: 1318802-26-4
PHPh₂(2-BF₃-Ph)

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; water

2: water; tetrahydrofuran

In tetrahydrofuran; methanol; water;
DOI:10.1021/om2004095