ethyl 4-(4-(5-((5-tert-butyloxazol-2-yl)methylthio)thiazol-2-ylcarbamoyloxy)phenoxy)butanoate

Base Information

Chemical Name:ethyl 4-(4-(5-((5-tert-butyloxazol-2-yl)methylthio)thiazol-2-ylcarbamoyloxy)phenoxy)butanoate
CAS No.:1133001-19-0
Molecular Formula:C₂₄H₂₉N₃O₆S₂
Molecular Weight:519.643
Hs Code.:

Synonyms:ethyl 4-(4-(5-((5-tert-butyloxazol-2-yl)methylthio)thiazol-2-ylcarbamoyloxy)phenoxy)butanoate

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Chemical Property of ethyl 4-(4-(5-((5-tert-butyloxazol-2-yl)methylthio)thiazol-2-ylcarbamoyloxy)phenoxy)butanoate

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Technology Process of ethyl 4-(4-(5-((5-tert-butyloxazol-2-yl)methylthio)thiazol-2-ylcarbamoyloxy)phenoxy)butanoate

There total 7 articles about ethyl 4-(4-(5-((5-tert-butyloxazol-2-yl)methylthio)thiazol-2-ylcarbamoyloxy)phenoxy)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 7693-46-1
4-Nitrophenyl chloroformate

: 166954-96-7
4-(4-hydroxy-phenoxy)-butyric acid ethyl ester

: 224436-97-9
2-amino-5-[[[5-(1,1-dimethylethyl)-2-oxazolyl]methyl]thio]-thiazole

: 1133001-19-0
ethyl 4-(4-(5-((5-tert-butyloxazol-2-yl)methylthio)thiazol-2-ylcarbamoyloxy)phenoxy)butanoate

Guidance literature:: 4-Nitrophenyl chloroformate; 2-amino-5-[[[5-(1,1-dimethylethyl)-2-oxazolyl]methyl]thio]-thiazole; With triethylamine; In dichloromethane; at 0 ℃; for 2h;

4-(4-hydroxy-phenoxy)-butyric acid ethyl ester; In dichloromethane; at 20 ℃;

Reference yield:

: 13547-70-1
1-chloro-3,3-dimethyl-butan-2-one

: 1133001-19-0
ethyl 4-(4-(5-((5-tert-butyloxazol-2-yl)methylthio)thiazol-2-ylcarbamoyloxy)phenoxy)butanoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium azide / acetone / 25 °C

2.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / methanol

3.1: triethylamine / dichloromethane / 1.25 h / -10 - -5 °C

4.1: trichlorophosphate / 1 h / 105 °C

5.1: ethanol; sodium tetrahydroborate / acetone / 1 h / 20 °C

5.2: 1 h / Reflux

6.1: triethylamine / dichloromethane / 2.25 h / 0 - 5 °C / Inert atmosphere

6.2: 0 - 20 °C

With hydrogenchloride; sodium tetrahydroborate; sodium azide; ethanol; hydrogen; triethylamine; trichlorophosphate; palladium 10% on activated carbon; In methanol; dichloromethane; acetone;

Reference yield:

: 76779-98-1
1-azido-3,3-dimethyl-2-butanone

: 1133001-19-0
ethyl 4-(4-(5-((5-tert-butyloxazol-2-yl)methylthio)thiazol-2-ylcarbamoyloxy)phenoxy)butanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / methanol

2.1: triethylamine / dichloromethane / 1.25 h / -10 - -5 °C

3.1: trichlorophosphate / 1 h / 105 °C

4.1: ethanol; sodium tetrahydroborate / acetone / 1 h / 20 °C

4.2: 1 h / Reflux

5.1: triethylamine / dichloromethane / 2.25 h / 0 - 5 °C / Inert atmosphere

5.2: 0 - 20 °C

With hydrogenchloride; sodium tetrahydroborate; ethanol; hydrogen; triethylamine; trichlorophosphate; palladium 10% on activated carbon; In methanol; dichloromethane; acetone;