2-[2-((1R,2R,6R)-2-Carboxy-2,6-dimethyl-6-vinyl-cyclohexyl)-ethyl]-4-isopropyl-benzoic acid

Base Information

• Chemical Name: 2-[2-((1R,2R,6R)-2-Carboxy-2,6-dimethyl-6-vinyl-cyclohexyl)-ethyl]-4-isopropyl-benzoic acid
• CAS No.: 6512-55-6
• Molecular Formula: C₂₃H₃₂O₄
• Molecular Weight: 372.505

Synonyms:2-[2-((1R,2R,6R)-2-Carboxy-2,6-dimethyl-6-vinyl-cyclohexyl)-ethyl]-4-isopropyl-benzoic acid

Chemical Property of 2-[2-((1R,2R,6R)-2-Carboxy-2,6-dimethyl-6-vinyl-cyclohexyl)-ethyl]-4-isopropyl-benzoic acid

Chemical Property:

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Technology Process of 2-[2-((1R,2R,6R)-2-Carboxy-2,6-dimethyl-6-vinyl-cyclohexyl)-ethyl]-4-isopropyl-benzoic acid

There total 2 articles about 2-[2-((1R,2R,6R)-2-Carboxy-2,6-dimethyl-6-vinyl-cyclohexyl)-ethyl]-4-isopropyl-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

2-[2-((1R,2R,6R)-2-Ethoxycarbonyl-2,6-dimethyl-6-vinyl-cyclohexyl)-ethyl]-4-isopropyl-benzoic acid ethyl ester (75399-78-9) → 2-[2-((1R,2R,6R)-2-Carboxy-2,6-dimethyl-6-vinyl-cyclohexyl)-ethyl]-4-isopropyl-benzoic acid (6512-55-6)

Guidance literature:

With potassium hydroxide; for 8h; Heating;

DOI:10.1021/jo01314a055

Reference yield:

→ 2-<2-(2t-Carboxyl-2r,6t-dimethyl-6-vinyl-cyclohexyl)-ethyl>-4-isopropyl-benzoesaeure-ethylester (6512-55-6)

Guidance literature:

2-<2-(2t-Carboxyl-2r,6t-dimethyl-6-vinyl-cyclohexyl)-ethyl>-4-isopropyl-benzoesaeure-ethylester (3c), NaOH, Erwaermen;

Reference yield: 35.0%

2-[2-((1R,2R,6R)-2-Carboxy-2,6-dimethyl-6-vinyl-cyclohexyl)-ethyl]-4-isopropyl-benzoic acid (6512-55-6) → (1R,5S,9R)-9-[2-(3-Isopropyl-phenyl)-ethyl]-1,4,5-trimethyl-3-oxa-bicyclo[3.3.1]nonan-2-one (75399-81-4) + (1R,2R,3R)-2-[2-(3-Isopropyl-phenyl)-ethyl]-1,3-dimethyl-3-vinyl-cyclohexanecarboxylic acid (75399-79-0)

Guidance literature:

With copper(I) oxide; In quinoline; at 240 ℃; for 5h;

DOI:10.1021/jo01314a055

upstream raw materials:

2-[2-((1R,2R,6R)-2-Ethoxycarbonyl-2,6-dimethyl-6-vinyl-cyclohexyl)-ethyl]-4-isopropyl-benzoic acid ethyl ester

Downstream raw materials:

(1R,5S,9R)-9-[2-(3-Isopropyl-phenyl)-ethyl]-1,4,5-trimethyl-3-oxa-bicyclo[3.3.1]nonan-2-one

(1R,2R,3R)-2-[2-(3-Isopropyl-phenyl)-ethyl]-1,3-dimethyl-3-vinyl-cyclohexanecarboxylic acid

(1R,2R,3R)-2-[2-(3-Isopropyl-phenyl)-ethyl]-1,3-dimethyl-3-vinyl-cyclohexanecarboxylic acid methyl ester

(1R,2R,3S)-3-Formyl-2-[2-(3-isopropyl-phenyl)-ethyl]-1,3-dimethyl-cyclohexanecarboxylic acid methyl ester

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