4-isopropoxy-N-[4-isopropoxy-5-methoxy-2-((2-methoxyethoxy)methoxy)benzyl]-3-methoxybenzamide

Base Information

Chemical Name:4-isopropoxy-N-[4-isopropoxy-5-methoxy-2-((2-methoxyethoxy)methoxy)benzyl]-3-methoxybenzamide
CAS No.:1333109-49-1
Molecular Formula:C₂₆H₃₇NO₈
Molecular Weight:491.582
Hs Code.:

Synonyms:4-isopropoxy-N-[4-isopropoxy-5-methoxy-2-((2-methoxyethoxy)methoxy)benzyl]-3-methoxybenzamide

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Chemical Property of 4-isopropoxy-N-[4-isopropoxy-5-methoxy-2-((2-methoxyethoxy)methoxy)benzyl]-3-methoxybenzamide

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Technology Process of 4-isopropoxy-N-[4-isopropoxy-5-methoxy-2-((2-methoxyethoxy)methoxy)benzyl]-3-methoxybenzamide

There total 8 articles about 4-isopropoxy-N-[4-isopropoxy-5-methoxy-2-((2-methoxyethoxy)methoxy)benzyl]-3-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1333109-48-0
4-isopropoxy-5-methoxy-2-((2-methoxyethoxy)methoxy)benzylamine

: 3535-33-9
4-isopropyloxy-3-methoxybenzoic acid

: 1333109-49-1
4-isopropoxy-N-[4-isopropoxy-5-methoxy-2-((2-methoxyethoxy)methoxy)benzyl]-3-methoxybenzamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.bmc.2011.06.056

Reference yield:

: 4-isopropoxy-3-methoxybenzoic acid isopropyl ester

: 1333109-49-1
4-isopropoxy-N-[4-isopropoxy-5-methoxy-2-((2-methoxyethoxy)methoxy)benzyl]-3-methoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / ethanol; water / 4 h / Reflux

1.2: pH 3

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; In tetrahydrofuran; ethanol; water;
DOI:10.1016/j.bmc.2011.06.056

Reference yield:

: 51061-83-7
2,4-dihydroxy-5-methoxybenzaldehyde

: 1333109-49-1
4-isopropoxy-N-[4-isopropoxy-5-methoxy-2-((2-methoxyethoxy)methoxy)benzyl]-3-methoxybenzamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 4 h / 70 °C / Inert atmosphere

2.1: potassium carbonate / N,N-dimethyl-formamide / 0.25 h / 20 °C

2.2: 12 h / 20 °C

3.1: pyridine; hydroxylamine hydrochloride / ethanol / 1.5 h / 20 °C

4.1: sodium hydroxide / ethanol / 1.5 h / 20 °C

5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

With pyridine; hydroxylamine hydrochloride; sodium hydrogencarbonate; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.06.056