N-(α-phenyl-2-nitro-4,5-dimethoxybenzyloxycarbonyl)-2,6-dimethylpiperidine

Base Information

Chemical Name:N-(α-phenyl-2-nitro-4,5-dimethoxybenzyloxycarbonyl)-2,6-dimethylpiperidine
CAS No.:1220634-65-0
Molecular Formula:C₂₃H₂₈N₂O₆
Molecular Weight:428.485
Hs Code.:

Synonyms:N-(α-phenyl-2-nitro-4,5-dimethoxybenzyloxycarbonyl)-2,6-dimethylpiperidine

Suppliers and Price of N-(α-phenyl-2-nitro-4,5-dimethoxybenzyloxycarbonyl)-2,6-dimethylpiperidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(α-phenyl-2-nitro-4,5-dimethoxybenzyloxycarbonyl)-2,6-dimethylpiperidine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(α-phenyl-2-nitro-4,5-dimethoxybenzyloxycarbonyl)-2,6-dimethylpiperidine

There total 2 articles about N-(α-phenyl-2-nitro-4,5-dimethoxybenzyloxycarbonyl)-2,6-dimethylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 1220634-66-1
α-phenyl-2-nitro-4,5-dimethoxybenzyl-4-nitrophenylcarbonate

: 504-03-0
2.6-dimethylpiperidine

: 1220634-65-0
N-(α-phenyl-2-nitro-4,5-dimethoxybenzyloxycarbonyl)-2,6-dimethylpiperidine

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; In ISOPROPYLAMIDE; at 60 - 70 ℃; for 4h; Inert atmosphere;

Reference yield:

: 179104-60-0
α-phenyl-4,5-dimethoxy-2-nitrobenzyl alcohol

: 1220634-65-0
N-(α-phenyl-2-nitro-4,5-dimethoxybenzyloxycarbonyl)-2,6-dimethylpiperidine

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / ISOPROPYLAMIDE / 0 - 20 °C / Inert atmosphere; Cooling with ice

2: 1-hydroxy-7-aza-benzotriazole / ISOPROPYLAMIDE / 4 h / 60 - 70 °C / Inert atmosphere

With dmap; 1-hydroxy-7-aza-benzotriazole; triethylamine; In ISOPROPYLAMIDE;