4-azido-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-4-deoxy-5-O-(4-methoxyphenyl)-L-arabinitol

Base Information

Chemical Name:4-azido-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-4-deoxy-5-O-(4-methoxyphenyl)-L-arabinitol
CAS No.:1206111-37-6
Molecular Formula:C₂₅H₃₇N₃O₅Si
Molecular Weight:487.671
Hs Code.:

Synonyms:4-azido-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-4-deoxy-5-O-(4-methoxyphenyl)-L-arabinitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-azido-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-4-deoxy-5-O-(4-methoxyphenyl)-L-arabinitol

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Technology Process of 4-azido-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-4-deoxy-5-O-(4-methoxyphenyl)-L-arabinitol

There total 1 articles about 4-azido-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-4-deoxy-5-O-(4-methoxyphenyl)-L-arabinitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1206111-82-1
C₁₉H₂₃N₃O₅

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1206111-37-6
4-azido-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-4-deoxy-5-O-(4-methoxyphenyl)-L-arabinitol

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 14h;
DOI:10.1002/ejoc.200900971

Reference yield: 96.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1206111-37-6
4-azido-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-4-deoxy-5-O-(4-methoxyphenyl)-L-arabinitol

: 1206111-51-4
3-O-benzyl-1-O-(tert-butyldimethylsilyl)-4-[(tert-butyloxycarbonyl)amino]-4-deoxy-5-O-(4-methoxyphenyl)-L-arabinitol

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 16h; under 750.075 Torr;
DOI:10.1002/ejoc.200900971

Reference yield:

: 136918-14-4,85-41-6
phthalimide

: 1206111-37-6
4-azido-3-O-benzyl-1-O-(tert-butyldimethylsilyl)-4-deoxy-5-O-(4-methoxyphenyl)-L-arabinitol

: 1206111-84-3
C₃₃H₄₀N₄O₆Si

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 14h;
DOI:10.1002/ejoc.200900971