5-(2-aminophenyl)-3H-1,3,4-thiadiazole-2-thione

Base Information

Chemical Name:5-(2-aminophenyl)-3H-1,3,4-thiadiazole-2-thione
CAS No.:51805-88-0
Molecular Formula:C₈H₇N₃S₂
Molecular Weight:209.296
Hs Code.:
ChEMBL ID:CHEMBL1484500
DSSTox Substance ID:DTXSID801333731

Synonyms:5-(2-aminophenyl)-3H-1,3,4-thiadiazole-2-thione;MLS000772657;CHEMBL1484500;SCHEMBL11025136;DTXSID801333731;HMS2703L09;AKOS034476265;51805-88-0;SMR000344675;2-(2-aminophenyl)-5-mercapto-1,3,4-thiadiazole;5-(2-aminophenyl)-1,3,4-thiadiazol-2(3h)-thione;Z57990369

Suppliers and Price of 5-(2-aminophenyl)-3H-1,3,4-thiadiazole-2-thione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 5-(2-aminophenyl)-3H-1,3,4-thiadiazole-2-thione

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:209.00813958
Heavy Atom Count:13
Complexity:252

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C2=NNC(=S)S2)N

Technology Process of 5-(2-aminophenyl)-3H-1,3,4-thiadiazole-2-thione

There total 5 articles about 5-(2-aminophenyl)-3H-1,3,4-thiadiazole-2-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 74037-19-7
N₂-(2-aminobenzoyl)thiosemicarbazide

: 51805-88-0
5-(2'-aminophenyl)-1,3,4-thiadiazole-2-thiol

Guidance literature:: With carbon disulfide; potassium hydroxide; In ethanol; at 75 - 80 ℃; for 5h;
DOI:10.13005/ojc/320528

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 36075-44-2
quinazolin-4-ylhydrazine

: 51805-88-0
5-(2'-aminophenyl)-1,3,4-thiadiazole-2-thiol

Guidance literature:: With potassium hydroxide; In ethanol; water; for 3h; Heating;
DOI:10.1021/jo00930a050

Reference yield:

: 87-25-2
2-ethoxycarbonylaniline

: 51805-88-0
5-(2'-aminophenyl)-1,3,4-thiadiazole-2-thiol

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / 20 h / 90 °C

2: hydrogenchloride / ethanol / 14 h / 80 °C

3: carbon disulfide; potassium hydroxide / ethanol / 5 h / 75 - 80 °C

With hydrogenchloride; carbon disulfide; hydrazine hydrate; potassium hydroxide; In ethanol;
DOI:10.13005/ojc/320528