C₃₁H₃₁N₂O⁽¹⁺⁾*Cl^(1-)

Base Information

Chemical Name:C₃₁H₃₁N₂O⁽¹⁺⁾*Cl^(1-)
CAS No.:1451930-04-3
Molecular Formula:C₃₁H₃₁N₂O*Cl
Molecular Weight:483.053
Hs Code.:

C<sub>31</sub>H<sub>31</sub>N<sub>2</sub>O<sup>(1+)</sup>*Cl<sup>(1-)</sup>

Synonyms:C₃₁H₃₁N₂O⁽¹⁺⁾*Cl^(1-)

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Chemical Property of C₃₁H₃₁N₂O⁽¹⁺⁾*Cl^(1-)

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Technology Process of C₃₁H₃₁N₂O⁽¹⁺⁾*Cl^(1-)

There total 4 articles about C₃₁H₃₁N₂O⁽¹⁺⁾*Cl^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1451929-67-1
C₃₀H₃₂N₂O

: 149-73-5
trimethyl orthoformate

: 1451930-04-3
C₃₁H₃₁N₂O⁽¹⁺⁾*Cl^(1-)

Guidance literature:: With ammonium chloride; In toluene; at 110 ℃; for 16h; Schlenk technique; Inert atmosphere;
DOI:10.1002/chem.201202318

Reference yield:

: 1451929-24-0
C₂₃H₂₆N₂

: 1451930-04-3
C₃₁H₃₁N₂O⁽¹⁺⁾*Cl^(1-)

Guidance literature:: Multi-step reaction with 2 steps

1: sodium cyanoborohydride; acetic acid / methanol; tetrahydrofuran / 20 °C / Inert atmosphere; Molecular sieve

2: ammonium chloride / toluene / 16 h / 110 °C / Schlenk technique; Inert atmosphere

With sodium cyanoborohydride; ammonium chloride; acetic acid; In tetrahydrofuran; methanol; toluene;
DOI:10.1002/chem.201202318

Reference yield:

: 29841-69-8
(S,S)-1,2-diphenyl-1,2-diaminoethane

: 1451930-04-3
C₃₁H₃₁N₂O⁽¹⁺⁾*Cl^(1-)

Guidance literature:: Multi-step reaction with 3 steps

1: 2-dicyclohexylphosphino-2′,6′-dimethoxybiphenyl; sodium butanolate; palladium diacetate / toluene / 48 h / 110 °C / Inert atmosphere; Schlenk technique

2: sodium cyanoborohydride; acetic acid / methanol; tetrahydrofuran / 20 °C / Inert atmosphere; Molecular sieve

3: ammonium chloride / toluene / 16 h / 110 °C / Schlenk technique; Inert atmosphere

With 2-dicyclohexylphosphino-2′,6′-dimethoxybiphenyl; palladium diacetate; sodium cyanoborohydride; ammonium chloride; acetic acid; sodium butanolate; In tetrahydrofuran; methanol; toluene; 1: |Buchwald-Hartwig Coupling;
DOI:10.1002/chem.201202318