C₂₉H₂₃NO₄

Base Information

Chemical Name:C₂₉H₂₃NO₄
CAS No.:1454786-31-2
Molecular Formula:C₂₉H₂₃NO₄
Molecular Weight:449.506
Hs Code.:

C<sub>29</sub>H<sub>23</sub>NO<sub>4</sub>

Synonyms:C₂₉H₂₃NO₄

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Chemical Property of C₂₉H₂₃NO₄

Chemical Property:

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Technology Process of C₂₉H₂₃NO₄

There total 3 articles about C₂₉H₂₃NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1454786-19-6
C₃₂H₂₇NO₄

: 1454786-31-2
C₂₉H₂₃NO₄

Guidance literature:: With (triphenylphosphine)gold(I) chloride; water; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; In dichloromethane; at 80 ℃; for 21h; Sealed tube;
DOI:10.1021/jo401390k

Reference yield:

: 276244-14-5
(+)-(3R,4S)-4-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]-3-hydroxy-3-(1-phenyl-1,2-propadienyl)-1-(p-methoxyphenyl)-2-azetidinone

: 1454786-31-2
C₂₉H₂₃NO₄

Guidance literature:: Multi-step reaction with 4 steps

1: acetyl chloride; sodium hydroxide; tetra-(n-butyl)ammonium iodide / water; dichloromethane / 24 h / 20 °C

2: N-Bromosuccinimide; silver(I) acetate / acetone / 3 h / 20 °C / Darkness

3: hydroxylamine hydrochloride; ethylamine; copper(l) chloride / water; dichloromethane; methanol / 3 h / 0 °C

4: (triphenylphosphine)gold(I) chloride; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; water / dichloromethane / 21 h / 80 °C / Sealed tube

With N-Bromosuccinimide; (triphenylphosphine)gold(I) chloride; hydroxylamine hydrochloride; water; silver(I) acetate; silver trifluoromethanesulfonate; tetra-(n-butyl)ammonium iodide; toluene-4-sulfonic acid; ethylamine; acetyl chloride; copper(l) chloride; sodium hydroxide; In methanol; dichloromethane; water; acetone; 3: |Cadiot-Chodkiewicz Coupling;
DOI:10.1021/jo401390k

Reference yield:

: 1399843-03-8
C₂₄H₂₃NO₄

: 1454786-31-2
C₂₉H₂₃NO₄

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide; silver(I) acetate / acetone / 3 h / 20 °C / Darkness

2: hydroxylamine hydrochloride; ethylamine; copper(l) chloride / water; dichloromethane; methanol / 3 h / 0 °C

3: (triphenylphosphine)gold(I) chloride; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; water / dichloromethane / 21 h / 80 °C / Sealed tube

With N-Bromosuccinimide; (triphenylphosphine)gold(I) chloride; hydroxylamine hydrochloride; water; silver(I) acetate; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; ethylamine; copper(l) chloride; In methanol; dichloromethane; water; acetone; 2: |Cadiot-Chodkiewicz Coupling;
DOI:10.1021/jo401390k