Benzoic acid (1S,6S)-2-methyl-6-(1,1,2-trimethyl-propoxy)-cyclohex-2-enyl ester

Base Information

Chemical Name:Benzoic acid (1S,6S)-2-methyl-6-(1,1,2-trimethyl-propoxy)-cyclohex-2-enyl ester
CAS No.:207788-80-5
Molecular Formula:C₂₀H₂₈O₃
Molecular Weight:316.441
Hs Code.:

Synonyms:Benzoic acid (1S,6S)-2-methyl-6-(1,1,2-trimethyl-propoxy)-cyclohex-2-enyl ester

Suppliers and Price of Benzoic acid (1S,6S)-2-methyl-6-(1,1,2-trimethyl-propoxy)-cyclohex-2-enyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid (1S,6S)-2-methyl-6-(1,1,2-trimethyl-propoxy)-cyclohex-2-enyl ester

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Technology Process of Benzoic acid (1S,6S)-2-methyl-6-(1,1,2-trimethyl-propoxy)-cyclohex-2-enyl ester

There total 1 articles about Benzoic acid (1S,6S)-2-methyl-6-(1,1,2-trimethyl-propoxy)-cyclohex-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 65-85-0,8013-63-6
benzoic acid

: (1R,6S)-2-Methyl-6-(1,1,2-trimethyl-propoxy)-cyclohex-2-enol

: 207788-80-5
Benzoic acid (1S,6S)-2-methyl-6-(1,1,2-trimethyl-propoxy)-cyclohex-2-enyl ester

Guidance literature:: With tributylphosphine; diethylazodicarboxylate; In tetrahydrofuran; for 20h; Ambient temperature;
DOI:10.1055/s-1998-5931

Reference yield: 93.0%

: 207788-80-5
Benzoic acid (1S,6S)-2-methyl-6-(1,1,2-trimethyl-propoxy)-cyclohex-2-enyl ester

: 207788-82-7
(1S,6S)-2-Methyl-6-(1,1,2-trimethyl-propoxy)-cyclohex-2-enol

Guidance literature:: With sodium methylate; In methanol; for 46.5h; Ambient temperature;
DOI:10.1055/s-1998-5931

Reference yield:

: 207788-80-5
Benzoic acid (1S,6S)-2-methyl-6-(1,1,2-trimethyl-propoxy)-cyclohex-2-enyl ester

: 207788-84-9
3-Bromo-2-[(1R,6S)-2-methyl-6-(1,1,2-trimethyl-propoxy)-cyclohex-2-enyloxy]-phenol

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / NaOMe / methanol / 46.5 h / Ambient temperature

2: DEAD, Bu₃P / tetrahydrofuran / 12.5 h

3: TBAF / tetrahydrofuran / 9 h / Ambient temperature

With tributylphosphine; tetrabutyl ammonium fluoride; sodium methylate; diethylazodicarboxylate; In tetrahydrofuran; methanol;
DOI:10.1055/s-1998-5931