Benzyl 3-bromo-2-[((1R,6S)-6-thexyloxy-2-methylcyclohex-2-enyl)oxy]phenyl ether

Base Information

Chemical Name:Benzyl 3-bromo-2-[((1R,6S)-6-thexyloxy-2-methylcyclohex-2-enyl)oxy]phenyl ether
CAS No.:207788-88-3
Molecular Formula:C₂₆H₃₃BrO₃
Molecular Weight:473.45
Hs Code.:

Synonyms:Benzyl 3-bromo-2-[((1R,6S)-6-thexyloxy-2-methylcyclohex-2-enyl)oxy]phenyl ether

Suppliers and Price of Benzyl 3-bromo-2-[((1R,6S)-6-thexyloxy-2-methylcyclohex-2-enyl)oxy]phenyl ether

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Benzyl 3-bromo-2-[((1R,6S)-6-thexyloxy-2-methylcyclohex-2-enyl)oxy]phenyl ether

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzyl 3-bromo-2-[((1R,6S)-6-thexyloxy-2-methylcyclohex-2-enyl)oxy]phenyl ether

There total 6 articles about Benzyl 3-bromo-2-[((1R,6S)-6-thexyloxy-2-methylcyclohex-2-enyl)oxy]phenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 100-39-0
benzyl bromide

: 207788-84-9
3-Bromo-2-[(1R,6S)-2-methyl-6-(1,1,2-trimethyl-propoxy)-cyclohex-2-enyloxy]-phenol

: 207788-88-3
Benzyl 3-bromo-2-[((1R,6S)-6-thexyloxy-2-methylcyclohex-2-enyl)oxy]phenyl ether

Guidance literature:: With potassium carbonate; In acetone; for 5h;
DOI:10.1055/s-1998-5931

Reference yield:

: 2-Bromo-6-(1,1,2-trimethyl-propoxy)-phenol

: 207788-88-3
Benzyl 3-bromo-2-[((1R,6S)-6-thexyloxy-2-methylcyclohex-2-enyl)oxy]phenyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: DEAD, Bu₃P / tetrahydrofuran / 12.5 h

2: TBAF / tetrahydrofuran / 9 h / Ambient temperature

3: 51 percent / K₂CO₃ / acetone / 5 h

With tributylphosphine; tetrabutyl ammonium fluoride; potassium carbonate; diethylazodicarboxylate; In tetrahydrofuran; acetone;
DOI:10.1055/s-1998-5931

Reference yield:

: 207788-80-5
Benzoic acid (1S,6S)-2-methyl-6-(1,1,2-trimethyl-propoxy)-cyclohex-2-enyl ester

: 207788-88-3
Benzyl 3-bromo-2-[((1R,6S)-6-thexyloxy-2-methylcyclohex-2-enyl)oxy]phenyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / NaOMe / methanol / 46.5 h / Ambient temperature

2: DEAD, Bu₃P / tetrahydrofuran / 12.5 h

3: TBAF / tetrahydrofuran / 9 h / Ambient temperature

4: 51 percent / K₂CO₃ / acetone / 5 h

With tributylphosphine; tetrabutyl ammonium fluoride; sodium methylate; potassium carbonate; diethylazodicarboxylate; In tetrahydrofuran; methanol; acetone;
DOI:10.1055/s-1998-5931