2,4,6-trimethylphenyl-ferrocene

Base Information

Chemical Name:2,4,6-trimethylphenyl-ferrocene
CAS No.:98774-03-9
Molecular Formula:C₁₉H₂₀Fe
Molecular Weight:304.215
Hs Code.:

Synonyms:2,4,6-trimethylphenyl-ferrocene

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Chemical Property of 2,4,6-trimethylphenyl-ferrocene

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Technology Process of 2,4,6-trimethylphenyl-ferrocene

There total 1 articles about 2,4,6-trimethylphenyl-ferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1293-67-0
1,1’-dichloroferrocene

: 108-67-8
1,3,5-trimethyl-benzene

: 102-54-5,55404-68-7
ferrocene

: 98774-03-9
2,4,6-trimethylphenyl-ferrocene

: 98774-04-0
(C₅H₄C₆H₂(CH₃)3)2Fe

Guidance literature:: With aluminium trichloride; aluminium; In 1,2,5-trimethyl-benzene; 2 equiv. AlCl3, heated to 100°C, stirred under N2 for 5 h; cooled, added with stirring to ice-cold H2O, layers septd., aq. layer washed with ether and organic layer with H2O, dried (MgSO4), evapd., chromy. on alumina with light petroleum/CH2Cl2, rechromy. on silica, crystd.(MeOH or l. petroleum), elem. anal.;

Reference yield: 59.0%

: 165272-06-0
[(η-6-naphthalene) tricarbonyl manganese] BF4

: 98774-03-9
2,4,6-trimethylphenyl-ferrocene

: 217315-32-7
(C₅H₅)Fe(C₅H₄C₆H₂(CH₃)3)Mn(CO)3⁽¹⁺⁾*BF₄^(1-)=[(C₅H₅)Fe(C₅H₄C₆H₂(CH₃)3)Mn(CO)3]BF₄

: 217315-34-9
(C₅H₅)Fe(C₅H₄C₆H₂(CH₃)3)Fe(C₅H₄C₆H₂(CH₃)3)⁽¹⁺⁾*BF₄^(1-)=[(C₅H₅)Fe(C₅H₄C₆H₂(CH₃)3)Fe(C₅H₄C₆H₂(CH₃)3)]BF₄

Guidance literature:: In dichloromethane; N2-atmosphere; refluxing Mn-complex with 2 equiv. of Fe-complex for 2-3 h, cooling to room temp.; in air; filtration, crystn., dissoln. in CH2Cl2, crystn. on diffusion ofEt2O and hexane into soln., hand sepn.; elem. anal.;
DOI:10.1016/S0020-1693(98)00166-2