tropan-2β-yl toluene-p-sulphonate

Base Information

Chemical Name:tropan-2β-yl toluene-p-sulphonate
CAS No.:78386-47-7
Molecular Formula:C₁₅H₂₁NO₃S
Molecular Weight:295.403
Hs Code.:

Synonyms:tropan-2β-yl toluene-p-sulphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tropan-2β-yl toluene-p-sulphonate

Chemical Property:

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Technology Process of tropan-2β-yl toluene-p-sulphonate

There total 8 articles about tropan-2β-yl toluene-p-sulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 98-59-9
p-toluenesulfonyl chloride

: 13466-55-2,13466-56-3,31354-42-4,36127-15-8,36127-16-9,36127-54-5,45738-02-1,66634-13-7,125279-26-7
tropan-2β-ol

: 78386-47-7
tropan-2β-yl toluene-p-sulphonate

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 18h;
DOI:10.1039/P19810001346

Reference yield:

: 78477-91-5
8-methyl-8-azabicyclo[3.2.1]octan-2-one

: 78386-47-7
tropan-2β-yl toluene-p-sulphonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium, pentan-3-ol

2: 37 percent / sodium hydride / tetrahydrofuran / 18 h

With 2-pentanol; sodium; sodium hydride; In tetrahydrofuran;
DOI:10.1039/P19810001346

Reference yield:

: 13612-59-4
cyclohepta-2,4,6-triene-1-carbonitrile

: 78386-47-7
tropan-2β-yl toluene-p-sulphonate

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / 2-methyl-propan-2-ol / 24 h / 85 °C

2: 1.)conc. HCl, 2.) thionyl chloride / 1.) reflux, 6 h, 2.) heated, 2 h

3: 1.) 1.2 M sodium hypochlorite, sodium hydroxide, 2.) 5 M hydrochloric acid / 1.) methanol, -20 deg C, 15 min, to warm to room temperature, 1 h, 70 deg C, 15 min, 2.) reflux, 1.5 h

4: sodium, pentan-3-ol

5: 37 percent / sodium hydride / tetrahydrofuran / 18 h

With hydrogenchloride; sodium hydroxide; sodium hypochlorite; thionyl chloride; 2-pentanol; sodium; sodium hydride; In tetrahydrofuran; tert-butyl alcohol;
DOI:10.1039/P19810001346