5,6-diphenyl-3--1,2,4-triazine

Base Information

• Chemical Name: 5,6-diphenyl-3--1,2,4-triazine
• CAS No.: 171773-55-0
• Molecular Formula: C₁₈H₁₅N₃O₂S
• Molecular Weight: 337.402
• Mol file: 171773-55-0.mol

Synonyms:5,6-diphenyl-3--1,2,4-triazine

Chemical Property of 5,6-diphenyl-3--1,2,4-triazine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5,6-diphenyl-3--1,2,4-triazine

There total 2 articles about 5,6-diphenyl-3--1,2,4-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

3-(5,6-Diphenyl-[1,2,4]triazin-3-ylsulfanyl)-propionic acid ethyl ester → 5,6-diphenyl-3--1,2,4-triazine (171773-55-0)

Guidance literature:

With sodium hydroxide; In ethyl acetate; for 3h; Ambient temperature;

Reference yield: 34.0%

3-Bromopropionic acid (590-92-1) + 5,6-diphenyl-1,2,4-triazine-3-thiol (37469-24-2) → 5,6-diphenyl-3--1,2,4-triazine (171773-55-0)

Guidance literature:

With triethylamine; In acetone; Reflux;

DOI:10.1016/j.ejmech.2017.07.011

Reference yield:

2,3-Diaminonaphthalene (771-97-1) + 5,6-diphenyl-3--1,2,4-triazine (171773-55-0) → 2-[2-(5,6-Diphenyl-[1,2,4]triazin-3-ylsulfanyl)-ethyl]-1H-naphtho[2,3-d]imidazole

Guidance literature:

With PPA; at 70 - 80 ℃; for 8h;

upstream raw materials:

3-Bromopropionic acid

5,6-diphenyl-1,2,4-triazine-3-thiol