{2-[(S)-3-Phenyl-2-(3-trimethylsilanyl-prop-2-ynyloxycarbonylamino)-propionylamino]-acetylamino}-acetic acid prop-2-ynyl ester

Base Information

Chemical Name:{2-[(S)-3-Phenyl-2-(3-trimethylsilanyl-prop-2-ynyloxycarbonylamino)-propionylamino]-acetylamino}-acetic acid prop-2-ynyl ester
CAS No.:914468-14-7
Molecular Formula:C₂₃H₂₉N₃O₆Si
Molecular Weight:471.585
Hs Code.:

Synonyms:{2-[(S)-3-Phenyl-2-(3-trimethylsilanyl-prop-2-ynyloxycarbonylamino)-propionylamino]-acetylamino}-acetic acid prop-2-ynyl ester

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Chemical Property of {2-[(S)-3-Phenyl-2-(3-trimethylsilanyl-prop-2-ynyloxycarbonylamino)-propionylamino]-acetylamino}-acetic acid prop-2-ynyl ester

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Technology Process of {2-[(S)-3-Phenyl-2-(3-trimethylsilanyl-prop-2-ynyloxycarbonylamino)-propionylamino]-acetylamino}-acetic acid prop-2-ynyl ester

There total 3 articles about {2-[(S)-3-Phenyl-2-(3-trimethylsilanyl-prop-2-ynyloxycarbonylamino)-propionylamino]-acetylamino}-acetic acid prop-2-ynyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 914468-15-8
4-nitrophenyl 3-(trimethylsilyl)-2-propynyl carbonate

: propargyl L-phenylalanylglycylglycinate hydrochloride

: 914468-14-7
{2-[(S)-3-Phenyl-2-(3-trimethylsilanyl-prop-2-ynyloxycarbonylamino)-propionylamino]-acetylamino}-acetic acid prop-2-ynyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1021/ol061657d

Reference yield:

: L-phenylalanylglycylglycine hydrochloride

: 914468-14-7
{2-[(S)-3-Phenyl-2-(3-trimethylsilanyl-prop-2-ynyloxycarbonylamino)-propionylamino]-acetylamino}-acetic acid prop-2-ynyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: HCl / diethyl ether / 18 h / 20 °C

2: 1.38 g / Et₃N / CH₂Cl₂ / 18 h / 20 °C

With hydrogenchloride; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1021/ol061657d

Reference yield:

: 5272-36-6
3-trimethylsilyl-2-propyn-1-ol

: 914468-14-7
{2-[(S)-3-Phenyl-2-(3-trimethylsilanyl-prop-2-ynyloxycarbonylamino)-propionylamino]-acetylamino}-acetic acid prop-2-ynyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / pyridine / CH₂Cl₂ / 36 h / 20 °C

2: 1.38 g / Et₃N / CH₂Cl₂ / 18 h / 20 °C

With pyridine; triethylamine; In dichloromethane;
DOI:10.1021/ol061657d