5-[3-(2,5-dichloro-4,6-dimethyl-1-oxy-pyridin-3-yl)-[1,2,4]oxadiazol-5-yl]-2-hydroxy-3-methoxy-1-nitrobenzene

Base Information

Chemical Name:5-[3-(2,5-dichloro-4,6-dimethyl-1-oxy-pyridin-3-yl)-[1,2,4]oxadiazol-5-yl]-2-hydroxy-3-methoxy-1-nitrobenzene
CAS No.:1402714-41-3
Molecular Formula:C₁₆H₁₂Cl₂N₄O₆
Molecular Weight:427.2
Hs Code.:

Synonyms:5-[3-(2,5-dichloro-4,6-dimethyl-1-oxy-pyridin-3-yl)-[1,2,4]oxadiazol-5-yl]-2-hydroxy-3-methoxy-1-nitrobenzene

Suppliers and Price of 5-[3-(2,5-dichloro-4,6-dimethyl-1-oxy-pyridin-3-yl)-[1,2,4]oxadiazol-5-yl]-2-hydroxy-3-methoxy-1-nitrobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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AK Scientific
4-[3-(2,5-Dichloro-4,6-dimethyl-1-oxidopyridin-1-ium-3-yl)-1,2,4-oxadiazol-5-yl]-2-methoxy-6-nitrophenol
1g
$ 1680.00

Total 2 raw suppliers

Chemical Property of 5-[3-(2,5-dichloro-4,6-dimethyl-1-oxy-pyridin-3-yl)-[1,2,4]oxadiazol-5-yl]-2-hydroxy-3-methoxy-1-nitrobenzene

Chemical Property:

Purity/Quality:

99.9% ^*data from raw suppliers

4-[3-(2,5-Dichloro-4,6-dimethyl-1-oxidopyridin-1-ium-3-yl)-1,2,4-oxadiazol-5-yl]-2-methoxy-6-nitrophenol ^*data from reagent suppliers

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Technology Process of 5-[3-(2,5-dichloro-4,6-dimethyl-1-oxy-pyridin-3-yl)-[1,2,4]oxadiazol-5-yl]-2-hydroxy-3-methoxy-1-nitrobenzene

There total 12 articles about 5-[3-(2,5-dichloro-4,6-dimethyl-1-oxy-pyridin-3-yl)-[1,2,4]oxadiazol-5-yl]-2-hydroxy-3-methoxy-1-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.8%

: 1391712-50-7
5-[3-(2,5-dichloro-4,6-dimethyl-pyridin-3-yl)-[1,2,4]oxadiazol-5-yl]-2-hydroxy-3-methoxy-1-nitrobenzene

: 1402714-41-3
5-[3-(2,5-dichloro-4,6-dimethyl-1-oxy-pyridin-3-yl)-[1,2,4]oxadiazol-5-yl]-2-hydroxy-3-methoxy-1-nitrobenzene

Guidance literature:: With urea hydrogen peroxide adduct; trifluoroacetic anhydride; In dichloromethane; at 5 - 25 ℃; Concentration; Temperature; Time; Large scale;

Reference yield:

: 121-34-6
3-methoxy-4-hydroxybenzoic acid

: 1402714-41-3
5-[3-(2,5-dichloro-4,6-dimethyl-1-oxy-pyridin-3-yl)-[1,2,4]oxadiazol-5-yl]-2-hydroxy-3-methoxy-1-nitrobenzene

Guidance literature:: Multi-step reaction with 4 steps

1: nitric acid; acetic acid / 10 - 23 °C

2: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 40 °C / Large scale

3: pyridine / 1,4-dioxane / 7 h / 10 - 115 °C

4: urea hydrogen peroxide adduct; trifluoroacetic anhydride / dichloromethane / 5 - 25 °C / Large scale

With pyridine; thionyl chloride; nitric acid; urea hydrogen peroxide adduct; acetic acid; N,N-dimethyl-formamide; trifluoroacetic anhydride; In 1,4-dioxane; dichloromethane;

Reference yield:

: 4-hydroxy-5-methoxy-3-nitrobenzoyl chloride

: 1402714-41-3
5-[3-(2,5-dichloro-4,6-dimethyl-1-oxy-pyridin-3-yl)-[1,2,4]oxadiazol-5-yl]-2-hydroxy-3-methoxy-1-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 1,4-dioxane / 7 h / 10 - 115 °C

2: urea hydrogen peroxide adduct; trifluoroacetic anhydride / dichloromethane / 5 - 25 °C / Large scale

With pyridine; urea hydrogen peroxide adduct; trifluoroacetic anhydride; In 1,4-dioxane; dichloromethane;