N-benzyl-triethylenetetramine-N,N',N'',N''',N'''-pentaacetamide

Base Information

Chemical Name:N-benzyl-triethylenetetramine-N,N',N'',N''',N'''-pentaacetamide
CAS No.:1058599-02-2
Molecular Formula:C₂₃H₃₉N₉O₅
Molecular Weight:521.62
Hs Code.:

Synonyms:N-benzyl-triethylenetetramine-N,N',N'',N''',N'''-pentaacetamide

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Chemical Property of N-benzyl-triethylenetetramine-N,N',N'',N''',N'''-pentaacetamide

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Technology Process of N-benzyl-triethylenetetramine-N,N',N'',N''',N'''-pentaacetamide

There total 1 articles about N-benzyl-triethylenetetramine-N,N',N'',N''',N'''-pentaacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1058598-87-0
pentaethyl N-benzyl-triethylenetetramine-N,N',N'',N''',N'''-pentaacetate

: 1058599-02-2
N-benzyl-triethylenetetramine-N,N',N'',N''',N'''-pentaacetamide

Guidance literature:: With ammonia; In methanol; at 20 ℃; for 216h;
DOI:10.1039/b803557a

Reference yield: 83.0%

: 10035-01-5
ytterbium(III) chloride hexahydrate

: 1058599-02-2
N-benzyl-triethylenetetramine-N,N',N'',N''',N'''-pentaacetamide

: 7732-18-5
water

: [Yb(N-benzyl-triethylenetetramine-N,N',N'',N''',N'''-pentaacetamide)]Cl₃*3H₂O

Guidance literature:: In methanol; mixt. was heated under reflux for 0.5 h; at room temp. propionitrile was added, soln. was filtered, ppt. washed with acetone and dried, ppt. was recrystd. from MeOH-propionitrile, driedand stored over silica; elem. anal.;
DOI:10.1039/b803557a

Reference yield: 79.0%

: europium(III) chloride hydrate

: 1058599-02-2
N-benzyl-triethylenetetramine-N,N',N'',N''',N'''-pentaacetamide

: (N-benzyl-triethylenetetramine-N,N',N'',N''',N'''-pentaacetamide)europium(III) chloride tetrahydrate

Guidance literature:: In methanol; Eu salt added to a suspn. of ligand, refluxed for 0.5 h; propionitrile added at room temp., filtered, crystd. for a few days, filtered, washed (acetone), dried, recrystd. (MeOH/propionitrile), dried over silica; elem. anal.;
DOI:10.1021/ic900652y