(E)-N,N'-bis(tert-butyloxycarbonyl)-N,N'-bis[(4-methylphenyl)sulfonyl]-3-hexene-1,6-diamine

Base Information

• Chemical Name: (E)-N,N'-bis(tert-butyloxycarbonyl)-N,N'-bis[(4-methylphenyl)sulfonyl]-3-hexene-1,6-diamine
• CAS No.: 1079308-79-4
• Molecular Formula: C₃₀H₄₂N₂O₈S₂
• Molecular Weight: 622.804

Synonyms:(E)-N,N'-bis(tert-butyloxycarbonyl)-N,N'-bis[(4-methylphenyl)sulfonyl]-3-hexene-1,6-diamine

Chemical Property of (E)-N,N'-bis(tert-butyloxycarbonyl)-N,N'-bis[(4-methylphenyl)sulfonyl]-3-hexene-1,6-diamine

Chemical Property:

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Technology Process of (E)-N,N'-bis(tert-butyloxycarbonyl)-N,N'-bis[(4-methylphenyl)sulfonyl]-3-hexene-1,6-diamine

There total 1 articles about (E)-N,N'-bis(tert-butyloxycarbonyl)-N,N'-bis[(4-methylphenyl)sulfonyl]-3-hexene-1,6-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

hex-3-yne-1,6-diol (85655-98-7) + N-[(tert-butoxy)carbonyl]-4-methylbenzenesulfonamide (18303-04-3) → (E)-N,N'-bis(tert-butyloxycarbonyl)-N,N'-bis[(4-methylphenyl)sulfonyl]-3-hexene-1,6-diamine (1079308-79-4)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1039/b806524a

Reference yield: 99.0%

(E)-N,N'-bis(tert-butyloxycarbonyl)-N,N'-bis[(4-methylphenyl)sulfonyl]-3-hexene-1,6-diamine (1079308-79-4) → N,N'-bis(4-methylphenyl)sulfonyl-3-hexene-1,6-diamine (1000205-59-3)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1039/b806524a

upstream raw materials:

hex-3-yne-1,6-diol

N-[(tert-butoxy)carbonyl]-4-methylbenzenesulfonamide

Downstream raw materials:

N,N'-bis(4-methylphenyl)sulfonyl-3-hexene-1,6-diamine

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