9-(2,6-dibromophenoxycarbonyl)-2,7-dimethoxy-10-(3-succinimidyloxycarbonylpropyl)acridinium Iodide

Base Information

Chemical Name:9-(2,6-dibromophenoxycarbonyl)-2,7-dimethoxy-10-(3-succinimidyloxycarbonylpropyl)acridinium Iodide
CAS No.:1332927-29-3
Molecular Formula:C₃₀H₂₅Br₂N₂O₈*I
Molecular Weight:828.25
Hs Code.:

Synonyms:9-(2,6-dibromophenoxycarbonyl)-2,7-dimethoxy-10-(3-succinimidyloxycarbonylpropyl)acridinium Iodide

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Chemical Property of 9-(2,6-dibromophenoxycarbonyl)-2,7-dimethoxy-10-(3-succinimidyloxycarbonylpropyl)acridinium Iodide

Chemical Property:

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Technology Process of 9-(2,6-dibromophenoxycarbonyl)-2,7-dimethoxy-10-(3-succinimidyloxycarbonylpropyl)acridinium Iodide

There total 7 articles about 9-(2,6-dibromophenoxycarbonyl)-2,7-dimethoxy-10-(3-succinimidyloxycarbonylpropyl)acridinium Iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.0%

: 1332927-30-6
2,6-dibromophenyl 2,7-dimethoxyacridine-9-carboxylate

: succinimidyl 4-iodobutanoate

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 1332927-29-3
9-(2,6-dibromophenoxycarbonyl)-2,7-dimethoxy-10-(3-succinimidyloxycarbonylpropyl)acridinium Iodide

Guidance literature:: In acetonitrile;

Reference yield:

: 104-94-9
4-methoxy-aniline

: 1332927-29-3
9-(2,6-dibromophenoxycarbonyl)-2,7-dimethoxy-10-(3-succinimidyloxycarbonylpropyl)acridinium Iodide

Guidance literature:: Multi-step reaction with 6 steps

1.1: copper(l) iodide; potassium carbonate; L-proline / dimethyl sulfoxide / 48 h / 90 °C

2.1: dichloromethane / 1 h / Reflux

2.2: 1 h / Reflux

3.1: potassium hydroxide / water / 72 h / Reflux

3.2: Cooling with ice

4.1: thionyl chloride / 3 h / Reflux

5.1: pyridine / 70 °C

6.1: 3 h / 150 °C / Inert atmosphere

With pyridine; copper(l) iodide; thionyl chloride; potassium carbonate; L-proline; potassium hydroxide; In dichloromethane; water; dimethyl sulfoxide;
DOI:10.1021/ja202221h

Reference yield:

: 696-62-8
para-iodoanisole

: 1332927-29-3
9-(2,6-dibromophenoxycarbonyl)-2,7-dimethoxy-10-(3-succinimidyloxycarbonylpropyl)acridinium Iodide

Guidance literature:: Multi-step reaction with 6 steps

1.1: copper(l) iodide; potassium carbonate; L-proline / dimethyl sulfoxide / 48 h / 90 °C

2.1: dichloromethane / 1 h / Reflux

2.2: 1 h / Reflux

3.1: potassium hydroxide / water / 72 h / Reflux

3.2: Cooling with ice

4.1: thionyl chloride / 3 h / Reflux

5.1: pyridine / 70 °C

6.1: 3 h / 150 °C / Inert atmosphere

With pyridine; copper(l) iodide; thionyl chloride; potassium carbonate; L-proline; potassium hydroxide; In dichloromethane; water; dimethyl sulfoxide;
DOI:10.1021/ja202221h