4-(but-2-yn-1-yloxy)-4-(2-((tert-butyldimethylsilyl)oxy)ethyl)cyclohexa-2,5-dienone

Base Information

Chemical Name:4-(but-2-yn-1-yloxy)-4-(2-((tert-butyldimethylsilyl)oxy)ethyl)cyclohexa-2,5-dienone
CAS No.:1448451-01-1
Molecular Formula:C₁₈H₂₈O₃Si
Molecular Weight:320.504
Hs Code.:

Synonyms:4-(but-2-yn-1-yloxy)-4-(2-((tert-butyldimethylsilyl)oxy)ethyl)cyclohexa-2,5-dienone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(but-2-yn-1-yloxy)-4-(2-((tert-butyldimethylsilyl)oxy)ethyl)cyclohexa-2,5-dienone

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Technology Process of 4-(but-2-yn-1-yloxy)-4-(2-((tert-butyldimethylsilyl)oxy)ethyl)cyclohexa-2,5-dienone

There total 1 articles about 4-(but-2-yn-1-yloxy)-4-(2-((tert-butyldimethylsilyl)oxy)ethyl)cyclohexa-2,5-dienone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

: 764-01-2
methyl propargyl alcohol

: 96013-76-2
4-[2-(tert-butyldimethylsilyloxy)ethyl]phenol

: 1448451-01-1
4-(but-2-yn-1-yloxy)-4-(2-((tert-butyldimethylsilyl)oxy)ethyl)cyclohexa-2,5-dienone

Guidance literature:: With [bis(acetoxy)iodo]benzene; at 0 - 20 ℃;
DOI:10.1021/ja404593c

Reference yield: 80.0%

: 1448451-01-1
4-(but-2-yn-1-yloxy)-4-(2-((tert-butyldimethylsilyl)oxy)ethyl)cyclohexa-2,5-dienone

: 93877-21-5
1,4-dibenzyloxybut-2-yne

: 4,5-bis((benzyloxy)methyl)-8a-(2-((tert-butyldimethylsilyl)oxy)ethyl)-3-methyl-2,2a1,5a,8a-tetrahydro-6H-naphtho[1,8-bc]furan-6-one

Guidance literature:: With bis(tri-t-butylphosphine)palladium⁽⁰⁾; In toluene; at 80 ℃; for 5h; Molecular sieve; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.tet.2020.131862