4,4'''''-diiodo-3,2',2'''',3'''''-tetramethoxy-[1,4';1',1'';4'',1''';4''',1'''';4'''',1''''']sexiphenyl

Base Information

• Chemical Name: 4,4'''''-diiodo-3,2',2'''',3'''''-tetramethoxy-[1,4';1',1'';4'',1''';4''',1'''';4'''',1''''']sexiphenyl
• CAS No.: 243465-09-0
• Molecular Formula: C₄₀H₃₂I₂O₄
• Molecular Weight: 830.501

Synonyms:4,4'''''-diiodo-3,2',2'''',3'''''-tetramethoxy-[1,4';1',1'';4'',1''';4''',1'''';4'''',1''''']sexiphenyl

Chemical Property of 4,4'''''-diiodo-3,2',2'''',3'''''-tetramethoxy-[1,4';1',1'';4'',1''';4''',1'''';4'''',1''''']sexiphenyl

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Technology Process of 4,4'''''-diiodo-3,2',2'''',3'''''-tetramethoxy-[1,4';1',1'';4'',1''';4''',1'''';4'''',1''''']sexiphenyl

There total 1 articles about 4,4'''''-diiodo-3,2',2'''',3'''''-tetramethoxy-[1,4';1',1'';4'',1''';4''',1'''';4'''',1''''']sexiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

4,4'-diiodo-3,3'-dimethoxylbiphenyl (92160-61-7) + 4,4'-biphenyldiboronic acid (4151-80-8) → 4,4'''''-diiodo-3,2',2'''',3'''''-tetramethoxy-[1,4';1',1'';4'',1''';4''',1'''';4'''',1''''']sexiphenyl (243465-09-0)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate;

DOI:10.1021/ja991133r

Reference yield: 35.0%

4-cyanophenylboronic acid (126747-14-6) + 4,4'''''-diiodo-3,2',2'''',3'''''-tetramethoxy-[1,4';1',1'';4'',1''';4''',1'''';4'''',1''''']sexiphenyl (243465-09-0) → C54H40N2O4 (243465-10-3)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate;

DOI:10.1021/ja991133r

Reference yield:

4,4'''''-diiodo-3,2',2'''',3'''''-tetramethoxy-[1,4';1',1'';4'',1''';4''',1'''';4'''',1''''']sexiphenyl (243465-09-0) → 4,4'''''-diiodo-[1,4';1',1'';4'',1''';4''',1'''';4'''',1''''']sexiphenyl-3,2',2'''',3'''''-tetraol

Guidance literature:

With boron tribromide;

DOI:10.1021/ja991133r

upstream raw materials:

4,4'-diiodo-3,3'-dimethoxylbiphenyl

4,4'-biphenyldiboronic acid

Downstream raw materials:

C₅₄H₄₀N₂O₄

(3,2'''',3'''''-tris-tert-butoxycarbonylmethoxy-4,4'''''-diiodo-[1,4';1',1'';4'',1''';4''',1'''';4'''',1''''']sexiphenyl-2'-yloxy)-acetic acid tert-butyl ester

(2',2''''',3''''''-tris-tert-butoxycarbonylmethoxy-4''''''-iodo-4-methoxy-[1,1';4',4'';1'',1''';4''',1'''';4'''',1''''';4''''',1'''''']septiphenyl-2''-yloxy)-acetic acid tert-butyl ester

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