Technology Process of Magnesium diamide
There total 2 articles about Magnesium diamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
ammonia;
formation of Mg(NH2)2 very slow;
- Guidance literature:
-
In
neat (no solvent);
High Pressure; loaded into autoclave; after pumping to residual pressure of about 1 Pa at 20°C over 30 min, charged with NH3 to pressure of 0.6-0.8 MPa;left for 30 min; heated to 300°C; held for 3 h; cooled to about 20°C; heated again; drawn from reactor in inert at./; monitored by X-ray diffraction;
DOI:10.1134/S0020168509080068
