2,5-dioxopyrrolidin-1-yl 3-(2,5-dimethyl-3,6-dioxocyclohexa-1,4-dienyl)-3-methylbutanoate

Base Information

Chemical Name:2,5-dioxopyrrolidin-1-yl 3-(2,5-dimethyl-3,6-dioxocyclohexa-1,4-dienyl)-3-methylbutanoate
CAS No.:1353713-44-6
Molecular Formula:C₁₇H₁₉NO₆
Molecular Weight:333.341
Hs Code.:

Synonyms:2,5-dioxopyrrolidin-1-yl 3-(2,5-dimethyl-3,6-dioxocyclohexa-1,4-dienyl)-3-methylbutanoate

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Chemical Property of 2,5-dioxopyrrolidin-1-yl 3-(2,5-dimethyl-3,6-dioxocyclohexa-1,4-dienyl)-3-methylbutanoate

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Technology Process of 2,5-dioxopyrrolidin-1-yl 3-(2,5-dimethyl-3,6-dioxocyclohexa-1,4-dienyl)-3-methylbutanoate

There total 5 articles about 2,5-dioxopyrrolidin-1-yl 3-(2,5-dimethyl-3,6-dioxocyclohexa-1,4-dienyl)-3-methylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 219938-55-3
3-(2,5-dimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)-3-methylbutanoic acid

: 1353713-44-6
2,5-dioxopyrrolidin-1-yl 3-(2,5-dimethyl-3,6-dioxocyclohexa-1,4-dienyl)-3-methylbutanoate

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja210048x

Reference yield:

: 137-18-8
2,5-Dimethyl-1,4-benzoquinone

: 1353713-44-6
2,5-dioxopyrrolidin-1-yl 3-(2,5-dimethyl-3,6-dioxocyclohexa-1,4-dienyl)-3-methylbutanoate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium dithionite / diethyl ether; water

2: methanesulfonic acid / 3 h / 70 °C / Inert atmosphere

3: N-Bromosuccinimide / water; acetonitrile / 1 h / 20 °C

4: dicyclohexyl-carbodiimide / dichloromethane / 1 h / 20 °C / Inert atmosphere

With N-Bromosuccinimide; sodium dithionite; methanesulfonic acid; dicyclohexyl-carbodiimide; In diethyl ether; dichloromethane; water; acetonitrile;
DOI:10.1021/ja210048x

Reference yield:

: 615-90-7
2,5-dimethylhydroquinone

: 1353713-44-6
2,5-dioxopyrrolidin-1-yl 3-(2,5-dimethyl-3,6-dioxocyclohexa-1,4-dienyl)-3-methylbutanoate

Guidance literature:: Multi-step reaction with 3 steps

1: methanesulfonic acid / 3 h / 70 °C / Inert atmosphere

2: N-Bromosuccinimide / water; acetonitrile / 1 h / 20 °C

3: dicyclohexyl-carbodiimide / dichloromethane / 1 h / 20 °C / Inert atmosphere

With N-Bromosuccinimide; methanesulfonic acid; dicyclohexyl-carbodiimide; In dichloromethane; water; acetonitrile;
DOI:10.1021/ja210048x