9-(4-methoxy)-5-(4'-nitrophenyl)-3H,13aH-quinolino[3,2-f][1,2,4]triazolo[4,3-b][1,2,4]triazepine

Base Information

Chemical Name:9-(4-methoxy)-5-(4'-nitrophenyl)-3H,13aH-quinolino[3,2-f][1,2,4]triazolo[4,3-b][1,2,4]triazepine
CAS No.:1236182-61-8
Molecular Formula:C₁₉H₁₃N₇O₃
Molecular Weight:387.357
Hs Code.:

Synonyms:9-(4-methoxy)-5-(4'-nitrophenyl)-3H,13aH-quinolino[3,2-f][1,2,4]triazolo[4,3-b][1,2,4]triazepine

Suppliers and Price of 9-(4-methoxy)-5-(4'-nitrophenyl)-3H,13aH-quinolino[3,2-f][1,2,4]triazolo[4,3-b][1,2,4]triazepine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 9-(4-methoxy)-5-(4'-nitrophenyl)-3H,13aH-quinolino[3,2-f][1,2,4]triazolo[4,3-b][1,2,4]triazepine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 9-(4-methoxy)-5-(4'-nitrophenyl)-3H,13aH-quinolino[3,2-f][1,2,4]triazolo[4,3-b][1,2,4]triazepine

There total 5 articles about 9-(4-methoxy)-5-(4'-nitrophenyl)-3H,13aH-quinolino[3,2-f][1,2,4]triazolo[4,3-b][1,2,4]triazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 957768-24-0
3,4-diamino-5-(p-nitrophenyl)-1,2,4-triazole

: 73568-29-3
2-chloro-6-methoxyquinolin-3-carboxaldehyde

: 1236182-61-8
9-(4-methoxy)-5-(4'-nitrophenyl)-3H,13aH-quinolino[3,2-f][1,2,4]triazolo[4,3-b][1,2,4]triazepine

Guidance literature:: With toluene-4-sulfonic acid; N,N-dimethyl-formamide; for 0.1h; Microwave irradiation;

Reference yield:

: 619-50-1
4-nitrobenzoic acid methyl ester

: 1236182-61-8
9-(4-methoxy)-5-(4'-nitrophenyl)-3H,13aH-quinolino[3,2-f][1,2,4]triazolo[4,3-b][1,2,4]triazepine

Guidance literature:: Multi-step reaction with 5 steps

1: hydrazine hydrate / ethanol / Reflux

2: hydrogenchloride / water / Heating

3: sulfuric acid

4: hydrazine hydrate / ethanol / Reflux

5: 0.08 h / Microwave irradiation; Ionic liquid

With hydrogenchloride; sulfuric acid; hydrazine hydrate; In ethanol; water;
DOI:10.1016/j.bmcl.2011.06.007

Reference yield:

: 836-16-8
1-(4-nitrobenzoyl)thiosemicarbazide

: 1236182-61-8
9-(4-methoxy)-5-(4'-nitrophenyl)-3H,13aH-quinolino[3,2-f][1,2,4]triazolo[4,3-b][1,2,4]triazepine

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid

2: hydrazine hydrate / ethanol / Reflux

3: 0.08 h / Microwave irradiation; Ionic liquid

With sulfuric acid; hydrazine hydrate; In ethanol;
DOI:10.1016/j.bmcl.2011.06.007