methyl(4-methyl-benzenethiolato){1,2-bis(diphenylphosphino)ethane}nickel

Base Information

Chemical Name:methyl(4-methyl-benzenethiolato){1,2-bis(diphenylphosphino)ethane}nickel
CAS No.:115981-42-5
Molecular Formula:C₃₄H₃₄NiP₂S
Molecular Weight:595.347
Hs Code.:

Synonyms:methyl(4-methyl-benzenethiolato){1,2-bis(diphenylphosphino)ethane}nickel

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Chemical Property of methyl(4-methyl-benzenethiolato){1,2-bis(diphenylphosphino)ethane}nickel

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Technology Process of methyl(4-methyl-benzenethiolato){1,2-bis(diphenylphosphino)ethane}nickel

There total 1 articles about methyl(4-methyl-benzenethiolato){1,2-bis(diphenylphosphino)ethane}nickel which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 31387-22-1
dimethylnickel{1,2-bis(diphenylphosphino)ethane}

: 106-45-6
para-thiocresol

: 115981-42-5
methyl(4-methyl-benzenethiolato){1,2-bis(diphenylphosphino)ethane}nickel

Guidance literature:: In toluene; byproducts: methane; Dropwise addn. of HSC6H4-p-CH3 to NiMe2(dpe) under protective gas (toluene, low temp.), evolution of CH4, stirring (room temp.),; filtn., washing (Et2O), drying (vacuo), elem. anal.;

Reference yield: 80.0%

: 115981-42-5
methyl(4-methyl-benzenethiolato){1,2-bis(diphenylphosphino)ethane}nickel

: 15793-01-8
Ni(CO)2{1,2-bis(diphenylphosphino)ethane}

: 10436-83-6
S-(4-methylphenyl) ethanethioate

Guidance literature:: With carbon monoxide; In dichloromethane; Addn. of CO (ambient pressure) to metal complex (CH2Cl2, room temp.), stirring (4 h).; Trap-to-trap distn., GLC anal.;