N₃-benzoyl-1-[(2'R,3'R,8'S)-2',3'-diphenyl-1',4'-dioxaspiro[4.5]dec-6'-en-8'-yl]uracil

Base Information

• Chemical Name: N₃-benzoyl-1-[(2'R,3'R,8'S)-2',3'-diphenyl-1',4'-dioxaspiro[4.5]dec-6'-en-8'-yl]uracil
• CAS No.: 1130727-82-0
• Molecular Formula: C₃₁H₂₆N₂O₅
• Molecular Weight: 506.558

Synonyms:N₃-benzoyl-1-[(2'R,3'R,8'S)-2',3'-diphenyl-1',4'-dioxaspiro[4.5]dec-6'-en-8'-yl]uracil

Chemical Property of N₃-benzoyl-1-[(2'R,3'R,8'S)-2',3'-diphenyl-1',4'-dioxaspiro[4.5]dec-6'-en-8'-yl]uracil

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Technology Process of N₃-benzoyl-1-[(2'R,3'R,8'S)-2',3'-diphenyl-1',4'-dioxaspiro[4.5]dec-6'-en-8'-yl]uracil

There total 1 articles about N₃-benzoyl-1-[(2'R,3'R,8'S)-2',3'-diphenyl-1',4'-dioxaspiro[4.5]dec-6'-en-8'-yl]uracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

3-N-benzoyluracil (2775-87-3) + (1R)-4,4-[(1R,2R)-(1,2-diphenylethylene)dioxy]-2-cyclohexenol (331268-68-9) → N3-benzoyl-1-[(2'R,3'R,8'S)-2',3'-diphenyl-1',4'-dioxaspiro[4.5]dec-6'-en-8'-yl]uracil (1130727-82-0)

Guidance literature:

With di-tert-butyl-diazodicarboxylate; triphenylphosphine; In tetrahydrofuran; at -10 - 20 ℃; Inert atmosphere;

DOI:10.1021/jo802492g

Reference yield: 89.0%

N3-benzoyl-1-[(2'R,3'R,8'S)-2',3'-diphenyl-1',4'-dioxaspiro[4.5]dec-6'-en-8'-yl]uracil (1130727-82-0) → N3-benzoyl-1-[(1'S)-4'-oxocyclohex-2'-en-1'-yl]uracil (1130727-83-1)

Guidance literature:

With water; trifluoroacetic acid; at 0 ℃; for 0.666667h; Inert atmosphere;

DOI:10.1021/jo802492g

upstream raw materials:

3-N-benzoyluracil

(1R)-4,4-[(1R,2R)-(1,2-diphenylethylene)dioxy]-2-cyclohexenol

Downstream raw materials:

N₃-benzoyl-1-[(1'S)-4'-oxocyclohex-2'-en-1'-yl]uracil

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