phenyl 2-azido-2-deoxy-4-O-p-methoxybenzyl-1-thio-3-O-triisopropylsilyl-D-glucopyranose

Base Information

Chemical Name:phenyl 2-azido-2-deoxy-4-O-p-methoxybenzyl-1-thio-3-O-triisopropylsilyl-D-glucopyranose
CAS No.:1338594-62-9
Molecular Formula:C₂₉H₄₃N₃O₅SSi
Molecular Weight:573.829
Hs Code.:

Synonyms:phenyl 2-azido-2-deoxy-4-O-p-methoxybenzyl-1-thio-3-O-triisopropylsilyl-D-glucopyranose

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Chemical Property of phenyl 2-azido-2-deoxy-4-O-p-methoxybenzyl-1-thio-3-O-triisopropylsilyl-D-glucopyranose

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Technology Process of phenyl 2-azido-2-deoxy-4-O-p-methoxybenzyl-1-thio-3-O-triisopropylsilyl-D-glucopyranose

There total 4 articles about phenyl 2-azido-2-deoxy-4-O-p-methoxybenzyl-1-thio-3-O-triisopropylsilyl-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₄₁N₃O₅SSi

: 1338594-62-9
phenyl 2-azido-2-deoxy-4-O-p-methoxybenzyl-1-thio-3-O-triisopropylsilyl-D-glucopyranose

Guidance literature:: With di-n-butylboryl trifluoromethanesulfonate; borane; In tetrahydrofuran; at 0 ℃; Product distribution / selectivity;

Reference yield:

: 171032-74-9
1,3,4,6-tetra-O-acetyl-2-azido-2-deoxy-D-glucopyranose

: 1338594-62-9
phenyl 2-azido-2-deoxy-4-O-p-methoxybenzyl-1-thio-3-O-triisopropylsilyl-D-glucopyranose

Guidance literature:: Multi-step reaction with 5 steps

1: boron trifluoride diethyl etherate / dichloromethane

2: sodium methylate; methanol

3: camphor-10-sulfonic acid / acetonitrile

4: N-ethyl-N,N-diisopropylamine / dichloromethane

5: di-n-butylboryl trifluoromethanesulfonate; borane / tetrahydrofuran / 0 °C

With methanol; di-n-butylboryl trifluoromethanesulfonate; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; borane; sodium methylate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; acetonitrile;

Reference yield:

: 2-azido-2-deoxy-D-glucose

: 1338594-62-9
phenyl 2-azido-2-deoxy-4-O-p-methoxybenzyl-1-thio-3-O-triisopropylsilyl-D-glucopyranose

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine

2: boron trifluoride diethyl etherate / dichloromethane

3: sodium methylate; methanol

4: camphor-10-sulfonic acid / acetonitrile

5: N-ethyl-N,N-diisopropylamine / dichloromethane

6: di-n-butylboryl trifluoromethanesulfonate; borane / tetrahydrofuran / 0 °C

With pyridine; methanol; di-n-butylboryl trifluoromethanesulfonate; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; borane; sodium methylate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; acetonitrile;