9,10-dihydro-9,10-(1,3-epidithio-2-methano-2-p-methoxyphenyl-1-oxide)-propanoanthracene

Base Information

Chemical Name:9,10-dihydro-9,10-(1,3-epidithio-2-methano-2-p-methoxyphenyl-1-oxide)-propanoanthracene
CAS No.:116195-00-7
Molecular Formula:C₂₂H₁₈O₂S₂
Molecular Weight:378.516
Hs Code.:

Synonyms:9,10-dihydro-9,10-(1,3-epidithio-2-methano-2-p-methoxyphenyl-1-oxide)-propanoanthracene

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Chemical Property of 9,10-dihydro-9,10-(1,3-epidithio-2-methano-2-p-methoxyphenyl-1-oxide)-propanoanthracene

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Technology Process of 9,10-dihydro-9,10-(1,3-epidithio-2-methano-2-p-methoxyphenyl-1-oxide)-propanoanthracene

There total 3 articles about 9,10-dihydro-9,10-(1,3-epidithio-2-methano-2-p-methoxyphenyl-1-oxide)-propanoanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 116194-99-1
9,10-Dihydro-9,10-(1,3-epidithio-2-methano-2-p-methoxyphenyl)propanoanthracene

: 116195-00-7
9,10-dihydro-9,10-(1,3-epidithio-2-methano-2-p-methoxyphenyl-1-oxide)-propanoanthracene

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/S0040-4020(01)87816-9

Reference yield:

: 46491-50-3
9,19-Dibromo-9,10-dihydroanthracene

: 116195-00-7
9,10-dihydro-9,10-(1,3-epidithio-2-methano-2-p-methoxyphenyl-1-oxide)-propanoanthracene

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) thiourea/KOH, 2.) H₂O/H₂SO₄ / 1.) ethanol, 0 deg C, 2.) ethanol, 0 deg C

2: BF₃*(C₂H₅)2O / CH₂Cl₂ / 0 °C

3: m-chloroperbenzoic acid / CH₂Cl₂ / 0 °C

With potassium hydroxide; sulfuric acid; boron trifluoride diethyl etherate; water; thiourea; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1016/S0040-4039(00)96937-5

Reference yield:

: 116194-98-0
9,10-Dihydro-9,10-dimercaptoanthracene

: 116195-00-7
9,10-dihydro-9,10-(1,3-epidithio-2-methano-2-p-methoxyphenyl-1-oxide)-propanoanthracene

Guidance literature:: Multi-step reaction with 2 steps

1: BF₃*(C₂H₅)2O / CH₂Cl₂ / 0 °C

2: m-chloroperbenzoic acid / CH₂Cl₂ / 0 °C

With boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1016/S0040-4039(00)96937-5