N,N-dimethyl-9-(4-fluorobenzyl)-8-(8-benzyloxyquinoline-7-carboxamido)adenine

Base Information

Chemical Name:N,N-dimethyl-9-(4-fluorobenzyl)-8-(8-benzyloxyquinoline-7-carboxamido)adenine
CAS No.:908255-49-2
Molecular Formula:C₃₁H₂₆FN₇O₂
Molecular Weight:547.592
Hs Code.:

Synonyms:N,N-dimethyl-9-(4-fluorobenzyl)-8-(8-benzyloxyquinoline-7-carboxamido)adenine

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Chemical Property of N,N-dimethyl-9-(4-fluorobenzyl)-8-(8-benzyloxyquinoline-7-carboxamido)adenine

Chemical Property:

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Technology Process of N,N-dimethyl-9-(4-fluorobenzyl)-8-(8-benzyloxyquinoline-7-carboxamido)adenine

There total 7 articles about N,N-dimethyl-9-(4-fluorobenzyl)-8-(8-benzyloxyquinoline-7-carboxamido)adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 908255-48-1
N,N-dimethyl-8-amino-9-(4-fluorobenzyl)adenine

: 908255-30-1
8-benzyloxyquinoline-7-carboxylic acid benzyl ester

: 908255-49-2
N,N-dimethyl-9-(4-fluorobenzyl)-8-(8-benzyloxyquinoline-7-carboxamido)adenine

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.bmc.2006.04.011

Reference yield:

: 908255-47-0
N,N-dimethyl-8-bromo-9-(4-fluorobenzyl)adenine

: 908255-49-2
N,N-dimethyl-9-(4-fluorobenzyl)-8-(8-benzyloxyquinoline-7-carboxamido)adenine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / dimethylformamide / 8 h / 80 °C

2: H₂ / Pd/C / methanol

3: 53 percent / NaH / dimethylformamide / 20 °C

With sodium azide; hydrogen; sodium hydride; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2006.04.011

Reference yield:

: [8-azido-9-(4-fluoro-benzyl)-9H-purin-6-yl]-dimethyl-amine

: 908255-49-2
N,N-dimethyl-9-(4-fluorobenzyl)-8-(8-benzyloxyquinoline-7-carboxamido)adenine

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / methanol

2: 53 percent / NaH / dimethylformamide / 20 °C

With hydrogen; sodium hydride; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2006.04.011